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CAS No.: | 7013-21-0 |
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Name: | 2-Chloro-9-methyl-9H-purin-6-amine |
Article Data: | 5 |
Molecular Structure: | |
Formula: | C6H6ClN5 |
Molecular Weight: | 183.6 |
Synonyms: | 9H-Purin-6-amine,2-chloro-9-methyl;6-Amino-2-chloro-9-methylpurine;2-chloro-9-methyl-9H-purin-6-ylamine;2-Chlor-9-methyladenin;2-Chloro-9-methyl-9H-purin-6-amine;2-Chlor-9-methyl-9H-purin-6-ylamin;2-Chloro-9-methyladenine; |
Density: | 1.79g/cm3 |
Boiling Point: | 315.6°Cat760mmHg |
Flash Point: | 144.6°C |
PSA: | 69.62000 |
LogP: | 1.18010 |
Conditions | Yield |
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With ammonium hydroxide In acetonitrile at 55℃; for 5.5h; | 82% |
Conditions | Yield |
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With potassium carbonate In N,N-dimethyl-formamide | |
With tetra(n-butyl)ammonium hydroxide In dichloromethane for 1h; |
2-Chloro-9-methyladenine
Conditions | Yield |
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With ethanol; ammonia |
Conditions | Yield |
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Multi-step reaction with 2 steps 1: N,N-diisopropylethylamine, NH3 / propan-1-ol / 20 h / Heating 2: K2CO3 / dimethylformamide View Scheme |
Conditions | Yield |
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Multi-step reaction with 2 steps 1: potassium carbonate / acetonitrile / 24 h / 20 °C 2: ammonium hydroxide / acetonitrile / 5.5 h / 55 °C View Scheme |
Conditions | Yield |
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at 155 - 160℃; for 3h; | 87% |
2-Chloro-9-methyladenine
8-bromo-2-chloro-9-methyl-9H-purin-6-amine
Conditions | Yield |
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With bromine; sodium acetate trihydrate In tetrahydrofuran; methanol; water at -10 - 20℃; for 0.5h; | 60% |
tyrosamine
2-Chloro-9-methyladenine
4-(2-((6-amino-9-methyl-9H-purin-2-yl)amino)ethyl)phenol
Conditions | Yield |
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With N-ethyl-N,N-diisopropylamine In dimethyl sulfoxide at 145℃; for 42h; | 32% |
2-Chloro-9-methyladenine
sodium ethanolate
2-ethoxy-9-methyl-9H-purin-6-ylamine
Conditions | Yield |
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With ethanol at 130℃; |
Conditions | Yield |
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With ammonia; sodium In diethyl ether for 0.5h; | A 47 % Spectr. B n/a |