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7078-98-0

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Basic Information
CAS No.: 7078-98-0
Name: 2,6-BIS(1,1-DIMETHYLETHYL)-4-(PHENYLMETHYLENE)-2,5-CYCLOHEXADIEN-1-ONE
Article Data: 55
Molecular Structure:
Molecular Structure of 7078-98-0 (2,6-BIS(1,1-DIMETHYLETHYL)-4-(PHENYLMETHYLENE)-2,5-CYCLOHEXADIEN-1-ONE)
Formula: C21H26 O
Molecular Weight: 294.437
Synonyms: 2,5-Cyclohexadien-1-one,4-benzylidene-2,6-di-tert-butyl- (7CI,8CI); 4-Benzylidene-2,6-di-tert-butyl-2,5-cyclohexadien-1-one;4-Benzylidene-2,6-di-tert-butyl-cyclohexa-2,5-dienone;4-Benzylidene-2,6-di-tert-butylcyclohex-2,5-dienone
Density: 1.03g/cm3
Melting Point: 74-75 °C
Boiling Point: 426.1°C at 760 mmHg
Flash Point: 183°C
Solubility: 5μg/L at 20℃
PSA: 17.07000
LogP: 5.59770
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Synthetic route
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(3,5-di-tert-butyl-4-hydroxyphenyl)phenylcarbinol

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2,6-di-tert-butyl-4-benzylidene-cyclohexa-2,5-dienone

Conditions
ConditionsYield
With chloro-trimethyl-silane In dichloromethane for 3h;81%
With acetic anhydride In toluene for 0.25h; Inert atmosphere; Schlenk technique;
128-39-2

2,6-di-tert-butylphenol

100-52-7

benzaldehyde

7078-98-0

2,6-di-tert-butyl-4-benzylidene-cyclohexa-2,5-dienone

Conditions
ConditionsYield
Stage #1: 2,6-di-tert-butylphenol; benzaldehyde With piperidine In toluene for 3h; Reflux;
Stage #2: With acetic anhydride In toluene at 110 - 125℃; for 0.5h;		79.1%
Stage #1: 2,6-di-tert-butylphenol; benzaldehyde With piperidine In toluene Reflux;
Stage #2: With acetic anhydride In toluene for 0.25h;		78%
With piperidine; zinc(II) chloride In toluene Reagent/catalyst; Reflux; Dean-Stark;77.39%
17330-09-5

2,6-di-tert-butyl-4-(phenyl-piperidin-1-yl-methyl)-phenol

7078-98-0

2,6-di-tert-butyl-4-benzylidene-cyclohexa-2,5-dienone

Conditions
ConditionsYield
With acetic anhydride at 120℃; for 0.05h; Microwave irradiation; Green chemistry;70.18%

2,6-di-tert-butylphenol

100-52-7

benzaldehyde

7078-98-0

2,6-di-tert-butyl-4-benzylidene-cyclohexa-2,5-dienone

Conditions
ConditionsYield
Stage #1: 2,6-di-tert-butylphenol; benzaldehyde With piperidine In toluene for 12h; Reflux; Inert atmosphere;
Stage #2: With acetic anhydride In toluene at 100℃; for 0.5h; Inert atmosphere;		70%
4973-27-7

4-benzyl-2,6-di-tert-butylphenol

7078-98-0

2,6-di-tert-butyl-4-benzylidene-cyclohexa-2,5-dienone

Conditions
ConditionsYield
With potassium hydroxide; potassium hexacyanoferrate(III) In benzene
591-51-5

phenyllithium

trans-benzylidenacetophenone

trans-benzylidenacetophenone

7078-98-0

2,6-di-tert-butyl-4-benzylidene-cyclohexa-2,5-dienone

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 59 percent / tetrahydrofuran; diethyl ether; cyclohexane
2: 81 percent / trimethylsilyl chloride / CH2Cl2 / 3 h
View Scheme
1620-98-0

3,5-di-t-butyl-4-hydroxybenzaldehyde

7078-98-0

2,6-di-tert-butyl-4-benzylidene-cyclohexa-2,5-dienone

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 59 percent / tetrahydrofuran; diethyl ether; cyclohexane
2: 81 percent / trimethylsilyl chloride / CH2Cl2 / 3 h
View Scheme

2,6-di-tert-butyl-4-(di-n-propylamino-phenyl-methyl)-phenol

7078-98-0

2,6-di-tert-butyl-4-benzylidene-cyclohexa-2,5-dienone

Conditions
ConditionsYield
at 114℃; under 10 - 250 Torr; for 4h; Product distribution / selectivity;

2,6-di-tert-butyl-4-(di-n-butylamino-phenyl-methyl)-phenol

7078-98-0

2,6-di-tert-butyl-4-benzylidene-cyclohexa-2,5-dienone

Conditions
ConditionsYield
at 110 - 130℃; under 30 Torr; for 3.5 - 5h; Product distribution / selectivity;
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2,6-di-tert-butylphenol

7078-98-0

2,6-di-tert-butyl-4-benzylidene-cyclohexa-2,5-dienone

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: piperidine / toluene / Inert atmosphere; Schlenk technique; Reflux
2: acetic anhydride / toluene / 0.25 h / Inert atmosphere; Schlenk technique
View Scheme
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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-13437180835

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  • 2,6-BIS(1,1-DIMETHYLETHYL)-4-(PHENYLMETHYLENE)-2,5-CYCLOHEXADIEN-1-ONE

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    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

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    China (Mainland)  |  Contact Details

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    China (Mainland)  |  Contact Details

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    Shanghai Chinqesen Biotechnology Co., Ltd. Company slogan:?Innovation, cooperation and win-win Company introduction:?Shanghai Chinqesen Biotechnology Co., Ltd. is a professional ph

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    China (Mainland)  |  Contact Details

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    Hunan Runhui Chem Co., Ltd. is a comprehensive Fine chemicals and Pharmaceuticals Intermediates supplier in China , Established in Changsha City of Hunan province registered capit

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:86-731-85570686

    Address:29 Floor,Changsheng Upper Strata,Furong District,China

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  • 2,6-Bis(1,1-dimethylethyl)-4-(phenylmethylene)-2,5-cyclohexadien-1-one

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    7078-98-0

    2,6-Bis(1,1-dimethylethyl)-4-(phenylmethylene)-2,5-cyclohexadien-1-one

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    factory?direct?sale Application:Fine chemical intermediates, used as the main raw material for the synthesis of various pesticides, medicines, surfactants, polymer monomers, and antifungal agents

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  •  Chemlyte Solutions

    China (Mainland)  |  Contact Details

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