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| CAS No.: | 765-09-3 |
|---|---|
| Name: | 1-Bromotridecane |
| Article Data: | 24 |
| Molecular Structure: | |
|
|
|
| Formula: | C13H27 Br |
| Molecular Weight: | 263.261 |
| Synonyms: | 1-Bromo-n-tridecane;1-Bromotridecane; NSC 87870; Tridecyl bromide; n-Tridecyl bromide |
| EINECS: | 212-138-0 |
| Density: | 1.03 |
| Melting Point: | 4-7 °C(lit.) |
| Boiling Point: | 148-150 °C10 mm Hg(lit.) |
| Flash Point: | 110 ºC |
| Appearance: | light yellow liquid |
| Hazard Symbols: |
|
| Risk Codes: | R22;R37/38;R41 |
| Safety: | Poison by intravenous route. When heated to decomposition it emits toxic vapors of Br−. |
| PSA: | 0.00000 |
| LogP: | 5.69230 |
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| Conditions | Yield |
|---|---|
| With bromine; mercury(II) oxide In tetrachloromethane for 1.5h; Heating; | 92% |
| With [bis(acetoxy)iodo]benzene; bromine In various solvent(s) for 22h; bromodecarboxylation; Heating; irradiation; | 79% |
| (i) TlOEt, (ii) Br2; Multistep reaction; | |
| With bromine; thallium (I) ethoxide 1.) hexane, 2.) reflux, 3 h; Yield given. Multistep reaction; | |
| Multi-step reaction with 2 steps 1: oxalyl dichloride; N,N-dimethyl-formamide 2: dmap; Bromotrichloromethane; 2-mercaptopyridine-1-oxide sodium salt / 4 h / Reflux View Scheme |
| Conditions | Yield |
|---|---|
| With carbon tetrabromide In dichloromethane at -30 - 20℃; | 88% |
| With hydrogen bromide at 100℃; | |
| With hydrogen bromide |
- 68975-76-8
formaldehyde ditridecylacetal
- 765-09-3
1-bromotridecane
| Conditions | Yield |
|---|---|
| With phosphorus pentabromide; benzene |
| Conditions | Yield |
|---|---|
| With hydrogen bromide; dihydrogen peroxide |
- 765-09-3
1-bromotridecane
| Conditions | Yield |
|---|---|
| With phosphorus pentabromide |
| Conditions | Yield |
|---|---|
| in Gegenwart von Peroxyden; |
- 68975-76-8
formaldehyde ditridecylacetal
- 7789-69-7
phosphorus pentabromide
- 71-43-2
benzene
- 765-09-3
1-bromotridecane
- 765-09-3
1-bromotridecane
| Conditions | Yield |
|---|---|
| With tetrachloromethane; bromine |
- 765-09-3
1-bromotridecane
| Conditions | Yield |
|---|---|
| With bromine | |
| With tetrachloromethane; bromine | |
| With bromine |
- 765-09-3
1-bromotridecane
| Conditions | Yield |
|---|---|
| With Trichloroethylene; bromine |
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Chemistry
Chemical Name: 1-Bromotridecane
IUPAC NAME: 1-Bromotridecane
CAS No.: 765-09-3
EINECS: 212-138-0
RTECS: YD3100000
Molecular Formula: C13H27Br
Molecular Weight: 263.26 g/mol
Melting Point: 4-7 °C(lit.)
Density: 1.027 g/cm3
Flash Point: 120.4 °C
Boiling Point: 292.3 °C at 760 mmHg
Following is the structure of 1-Bromotridecane (CAS No.765-09-3):
Product Categories about 1-Bromotridecane (CAS No.765-09-3) are Alkyl Bromides ; Monofunctional & alpha,omega-Bifunctional Alkanes ; Monofunctional Alkanes
The chemical synonymous of 1-Bromotridecane (CAS No.765-09-3) are 1-Bromo-Tridecan ; N-Tridecyl-1-Bromide ; Tridecane,1-Bromo- ; 1-Bromotridecane ; Tridecyl Bromide ; N-Tridecyl Bromide ; 1-Bromotridecane,99%
Toxicity Data With Reference
| 1. | ivn-mus LD50:180 mg/kg | CSLNX* U.S. Army Armament Research & Development Command, Chemical Systems Laboratory, NIOSH Exchange Chemicals. (Aberdeen Proving Ground, MD 21010) NX#03504 . |
Consensus Reports
Reported in EPA TSCA Inventory.
Safety Profile
Poison by intravenous route. When heated to decomposition it emits toxic vapors of Br−.
Hazard Codes: 
Xn
Risk Statements about 1-Bromotridecane (CAS No.765-09-3):
R22:Harmful if swallowed.
R41:Risk of serious damage to the eyes.
R37/38:Irritating to respiratory system and skin.
Safety Statements about 1-Bromotridecane (CAS No.765-09-3):
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.
S39:Wear eye / face protection.
Attention:
1. Storage: Keep container closed when not in use. Store in a tightly closed container. Store in a cool, dry, well-ventilated area away from incompatible substances.
2. Handling: Avoid ingestion and inhalation. Avoid contact with eyes, skin, and clothing. Wash thoroughly after handling. Remove contaminated clothing and wash before reuse. Use with adequate ventilation.