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Basic Information
| CAS No.: | 77086-21-6 |
|---|---|
| Name: | Dizocilpine |
| Article Data: | 3 |
| Molecular Structure: | |
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|
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| Formula: | C16H15N |
| Molecular Weight: | 221.302 |
| Synonyms: | Dizocilpine |
| Density: | 1.144g/cm3 |
| Melting Point: | 68.5-69° |
| Boiling Point: | 320.3°C at 760 mmHg |
| Flash Point: | 152.6°C |
| PSA: | 12.03000 |
| LogP: | 3.47930 |
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Synthetic route
- 159170-13-5
(5S,10R)-(+)-5-(bromomethyl)-10,11-dihydro-5H-dibenzo-[a,d]-cyclohepten-5,10-imine
- 77086-21-6
Dizocilpine
Conditions
| Conditions | Yield |
|---|---|
| With lithium triethylborohydride In tetrahydrofuran at 60℃; for 3h; | 85% |
- 380427-51-0
(5S,10R)-(+)-5-(hydroxymethyl)-10,11-dihydro-5H-dibenzo[a,d]-cyclohepten-5,10-imine
- 77086-21-6
Dizocilpine
Conditions
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1.1: HCO2Et 1.2: 81 percent / SOBr2; aq. HBr 2.1: 85 percent / LiBHEt3 / tetrahydrofuran / 3 h / 60 °C View Scheme |
- 77086-21-6
Dizocilpine
Conditions
| Conditions | Yield |
|---|---|
| Multi-step reaction with 4 steps 1.1: 85 percent / Bu3SnH; AIBN / benzene / 1.5 h / Heating 2.1: aq. NaOH / ethanol / Heating 2.2: 89 percent / LiAlH4 / tetrahydrofuran / 40 h 3.1: HCO2Et 3.2: 81 percent / SOBr2; aq. HBr 4.1: 85 percent / LiBHEt3 / tetrahydrofuran / 3 h / 60 °C View Scheme |
- 380427-50-9
(5S,10R)-(+)-N-carboxylic acid vinyl ester-5-cyano-10,11-dihydro-5H-dibenzo[a,d]-cyclopenten-5,10-imine
- 77086-21-6
Dizocilpine
Conditions
| Conditions | Yield |
|---|---|
| Multi-step reaction with 3 steps 1.1: aq. NaOH / ethanol / Heating 1.2: 89 percent / LiAlH4 / tetrahydrofuran / 40 h 2.1: HCO2Et 2.2: 81 percent / SOBr2; aq. HBr 3.1: 85 percent / LiBHEt3 / tetrahydrofuran / 3 h / 60 °C View Scheme |
- 77086-21-6
Dizocilpine
Conditions
| Conditions | Yield |
|---|---|
| With sulfuric acid; nitric acid; acetic acid for 104h; Ambient temperature; | A 3% B 80% |
- 77086-21-6
Dizocilpine
- 74-88-4
methyl iodide
- 1222094-08-7
N,5-dimethyl-10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5,10-imine methiodide
Conditions
| Conditions | Yield |
|---|---|
| In diethyl ether for 96h; Darkness; | 60% |
- 77086-21-6
Dizocilpine
Conditions
| Conditions | Yield |
|---|---|
| Multi-step reaction with 3 steps 1: 3 percent / sulfuric acid, glacial acetic acid, fumic nitric acid / 104 h / Ambient temperature 2: 90 percent / aq. NaHCO3 / CHCl3 / 36 h / Ambient temperature 3: 57 percent / H2 / 10percent Pd/C / ethyl acetate / 16 h / 2327.2 Torr / Ambient temperature View Scheme |
- 77086-21-6
Dizocilpine
Conditions
| Conditions | Yield |
|---|---|
| Multi-step reaction with 4 steps 1: 3 percent / sulfuric acid, glacial acetic acid, fumic nitric acid / 104 h / Ambient temperature 2: 90 percent / aq. NaHCO3 / CHCl3 / 36 h / Ambient temperature 3: 57 percent / H2 / 10percent Pd/C / ethyl acetate / 16 h / 2327.2 Torr / Ambient temperature 4: 95 percent / aq. NaHCO3 / CHCl3 / 0.17 h View Scheme |
- 77086-21-6
Dizocilpine
Conditions
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1: 3 percent / sulfuric acid, glacial acetic acid, fumic nitric acid / 104 h / Ambient temperature 2: 90 percent / aq. NaHCO3 / CHCl3 / 36 h / Ambient temperature View Scheme |
- 77086-21-6
Dizocilpine
Conditions
| Conditions | Yield |
|---|---|
| Multi-step reaction with 5 steps 1: 3 percent / sulfuric acid, glacial acetic acid, fumic nitric acid / 104 h / Ambient temperature 2: 90 percent / aq. NaHCO3 / CHCl3 / 36 h / Ambient temperature 3: 57 percent / H2 / 10percent Pd/C / ethyl acetate / 16 h / 2327.2 Torr / Ambient temperature 4: 95 percent / aq. NaHCO3 / CHCl3 / 0.17 h 5: 75 percent / HCl (gas) / diethyl ether / 1 h / 0 - 20 °C View Scheme |
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Dizocilpine
