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CAS No.: | 796-77-0 |
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Name: | 4-[2-(diethylamino)ethoxy]benzophenone |
Article Data: | 6 |
Molecular Structure: | |
Formula: | C19H23 N O2 |
Molecular Weight: | 297.397 |
Synonyms: | Benzophenone,4-[2-(diethylamino)ethoxy]- (6CI,7CI,8CI); 4-(b-Diethylaminoethoxy)benzophenone; 4-[2-(Diethylamino)ethoxy]benzophenone |
Density: | 1.057g/cm3 |
Boiling Point: | 430.1°C at 760 mmHg |
Flash Point: | 213.9°C |
PSA: | 29.54000 |
LogP: | 3.63820 |
2-chloro-N,N-diethylethylamine hydrochloride
4-Hydroxybenzophenone
4-[2-(N,N-diethylamino)ethoxy]benzophenone
Conditions | Yield |
---|---|
With potassium carbonate In acetone for 6h; Heating; | 97% |
With tetrabutylammomium bromide In acetone at 30 - 40℃; for 4.16667h; | 8.32 g |
2-(diethylamino)ethyl chloride
4-Hydroxybenzophenone
4-[2-(N,N-diethylamino)ethoxy]benzophenone
Conditions | Yield |
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(i) Na, (ii) /BRN= 605300/; Multistep reaction; |
4-[2-(N,N-diethylamino)ethoxy]benzophenone
Conditions | Yield |
---|---|
With water-d2; magnesium; ethylene dibromide In tetrahydrofuran at 70℃; for 2h; Inert atmosphere; Schlenk technique; | 51% |
With water-d2; magnesium; ethylene dibromide In tetrahydrofuran | 51% |
p-benzyloxybenzaldehyde
4-[2-(N,N-diethylamino)ethoxy]benzophenone
1-<-4-<2-(diethylamino)ethoxy>phenyl>-1-phenyl-2-<(4-benzyloxy)phenyl>-2-hydroxyethene
Conditions | Yield |
---|---|
With titanium tetrachloride; zinc In tetrahydrofuran 1) reflux, 2 h, 2) r.t.; | 49% |
Conditions | Yield |
---|---|
With titanium tetrachloride; zinc In 1,4-dioxane for 4h; Heating; | 40% |
3-methoxy-4-(phenylmethoxy)benzaldehyde
4-[2-(N,N-diethylamino)ethoxy]benzophenone
1-<4-<2-(diethylamino)ethoxy>phenyl>-1-phenyl-2-hydroxy-2-<3-methoxy-4-(benzyloxy)phenyl>ethene
Conditions | Yield |
---|---|
With titanium tetrachloride; zinc In tetrahydrofuran 1) reflux, 2 h, 2) r.t.; | 36% |
4-[2-(N,N-diethylamino)ethoxy]benzophenone
vinylmagnesium chloride
1-[4-(2-Diethylamino-ethoxy)-phenyl]-1-phenyl-prop-2-en-1-ol
Conditions | Yield |
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In tetrahydrofuran |
4-[2-(N,N-diethylamino)ethoxy]benzophenone
ethylmagnesium bromide
4-(β-diethylaminoethoxy)-α-ethyl-benzhydrol
Conditions | Yield |
---|---|
In diethyl ether |
Dimethyl 1-Chloro-1-phenylmethanephosphonate
4-[2-(N,N-diethylamino)ethoxy]benzophenone
clomiphene
Conditions | Yield |
---|---|
With tert.-butyl lithium 1.) THF/pentane, -78 deg C, 30 min; 2.) THF, reflux; Yield given. Multistep reaction; |
ethyl bromide
4-[2-(N,N-diethylamino)ethoxy]benzophenone
4-(β-diethylaminoethoxy)-α-ethyl-benzhydrol
Conditions | Yield |
---|---|
With magnesium | |
With magnesium |