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796-77-0

Basic Information
CAS No.: 796-77-0
Name: 4-[2-(diethylamino)ethoxy]benzophenone
Article Data: 6
Molecular Structure:
Molecular Structure of 796-77-0 (4-[2-(diethylamino)ethoxy]benzophenone)
Formula: C19H23 N O2
Molecular Weight: 297.397
Synonyms: Benzophenone,4-[2-(diethylamino)ethoxy]- (6CI,7CI,8CI); 4-(b-Diethylaminoethoxy)benzophenone; 4-[2-(Diethylamino)ethoxy]benzophenone
Density: 1.057g/cm3
Boiling Point: 430.1°C at 760 mmHg
Flash Point: 213.9°C
PSA: 29.54000
LogP: 3.63820
Synthetic route
869-24-9

2-chloro-N,N-diethylethylamine hydrochloride

1137-42-4

4-Hydroxybenzophenone

796-77-0

4-[2-(N,N-diethylamino)ethoxy]benzophenone

Conditions
ConditionsYield
With potassium carbonate In acetone for 6h; Heating;97%
With tetrabutylammomium bromide In acetone at 30 - 40℃; for 4.16667h;8.32 g
100-35-6

2-(diethylamino)ethyl chloride

1137-42-4

4-Hydroxybenzophenone

796-77-0

4-[2-(N,N-diethylamino)ethoxy]benzophenone

Conditions
ConditionsYield
(i) Na, (ii) /BRN= 605300/; Multistep reaction;
796-77-0

4-[2-(N,N-diethylamino)ethoxy]benzophenone

C19H24(2)HNO2

Conditions
ConditionsYield
With water-d2; magnesium; ethylene dibromide In tetrahydrofuran at 70℃; for 2h; Inert atmosphere; Schlenk technique;51%
With water-d2; magnesium; ethylene dibromide In tetrahydrofuran51%
4397-53-9

p-benzyloxybenzaldehyde

796-77-0

4-[2-(N,N-diethylamino)ethoxy]benzophenone

117095-62-2

1-<-4-<2-(diethylamino)ethoxy>phenyl>-1-phenyl-2-<(4-benzyloxy)phenyl>-2-hydroxyethene

Conditions
ConditionsYield
With titanium tetrachloride; zinc In tetrahydrofuran 1) reflux, 2 h, 2) r.t.;49%
1007-32-5

benzyl ethyl ketone

796-77-0

4-[2-(N,N-diethylamino)ethoxy]benzophenone

2-benzyl-1-phenyl-1-[4-(diethylaminoethoxy)phenyl]but-1-ene

Conditions
ConditionsYield
With titanium tetrachloride; zinc In 1,4-dioxane for 4h; Heating;40%
2426-87-1

3-methoxy-4-(phenylmethoxy)benzaldehyde

796-77-0

4-[2-(N,N-diethylamino)ethoxy]benzophenone

117095-63-3

1-<4-<2-(diethylamino)ethoxy>phenyl>-1-phenyl-2-hydroxy-2-<3-methoxy-4-(benzyloxy)phenyl>ethene

Conditions
ConditionsYield
With titanium tetrachloride; zinc In tetrahydrofuran 1) reflux, 2 h, 2) r.t.;36%
796-77-0

4-[2-(N,N-diethylamino)ethoxy]benzophenone

3536-96-7

vinylmagnesium chloride

56431-04-0

1-[4-(2-Diethylamino-ethoxy)-phenyl]-1-phenyl-prop-2-en-1-ol

Conditions
ConditionsYield
In tetrahydrofuran
796-77-0

4-[2-(N,N-diethylamino)ethoxy]benzophenone

925-90-6

ethylmagnesium bromide

56431-20-0

4-(β-diethylaminoethoxy)-α-ethyl-benzhydrol

Conditions
ConditionsYield
In diethyl ether
16965-75-6

Dimethyl 1-Chloro-1-phenylmethanephosphonate

796-77-0

4-[2-(N,N-diethylamino)ethoxy]benzophenone

911-45-5

clomiphene

Conditions
ConditionsYield
With tert.-butyl lithium 1.) THF/pentane, -78 deg C, 30 min; 2.) THF, reflux; Yield given. Multistep reaction;
74-96-4

ethyl bromide

796-77-0

4-[2-(N,N-diethylamino)ethoxy]benzophenone

56431-20-0

4-(β-diethylaminoethoxy)-α-ethyl-benzhydrol

Conditions
ConditionsYield
With magnesium
With magnesium
Downstream Products
911-45-5
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