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| CAS No.: | 85329-86-8 |
|---|---|
| Name: | Desethylcarbamoyl Cabergoline |
| Article Data: | 3 |
| Molecular Structure: | |
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| Formula: | C23H32N4O |
| Molecular Weight: | 380.533 |
| Synonyms: | Cabergoline specified impurity D;Cabergoline related compound D;Desethylcarbamoyl Cabergoline;UNII-114UFJ65CL; |
| Density: | 1.13g/cm3 |
| Melting Point: | 188-190°C |
| Boiling Point: | 607.7°C at 760 mmHg |
| Flash Point: | 321.3°C |
| PSA: | 54.86000 |
| LogP: | 3.53020 |
- 958254-66-51H-Imidazo[4,5-b]pyridine-2-carboxaldehyde, 1-methyl-, hydrochloride
- 99170-93-1N-Methyl-2-oxazolamine
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- 90221-55-92-bromo-5-methylbenzaldehyde
- 885590-99-82,3-DIFLUORO-4-IODOBENZALDEHYDE
- 97730-31-9(S)-4'-(2-Methylbutyl)Biphenyl-4-Carbonitrile
- 926293-55-26-Bromo-2-methylpyridine-3-carboxaldehyde
- 911112-05-55-Iodo-3-(trifluoromethyl)-2-pyridinamine
- 886364-50-71-(5-Bromo-2-pyridinyl)-2,2,2-trifluoroethanone
- 72821-79-5
methyl (6aR,9R,10aR)-7-allyl-4,6,6a,7,8,9,10,10a-octahydroindolo[4,3-fg]quinoline-9-carboxylate
- 109-55-7
1-amino-3-(dimethylamino)propane
- 85329-86-8
(6aR,9R,10aR)-7-allyl-N-[3-(dimethylamino)propyl]-4,6,6a,7,8,9,10,10a-octahydroindolo[4,3-fg]quinoline-9-carboxamide
| Conditions | Yield |
|---|---|
| In acetic acid Heating; | 85% |
| With 2-hydroxypyridin In ethylene glycol at 100℃; for 18h; | 85% |
| With acetic acid for 24h; Reflux; | 74% |
- 3006-19-7, 5143-94-2, 35470-53-2, 77842-02-5, 87247-99-2, 96648-31-6, 96648-32-7
9,10-dihydrolysergic acid methyl ester
- 85329-86-8
(6aR,9R,10aR)-7-allyl-N-[3-(dimethylamino)propyl]-4,6,6a,7,8,9,10,10a-octahydroindolo[4,3-fg]quinoline-9-carboxamide
| Conditions | Yield |
|---|---|
| Multi-step reaction with 4 steps 1: dmap / dichloromethane / 16 h / Reflux; Inert atmosphere 2: zinc / methanol; acetic acid / 1.08 h / 20 °C 3: potassium carbonate / N,N-dimethyl-formamide / 2.5 h / 35 °C 4: acetic acid / 24 h / Reflux View Scheme |
- 80993-64-2
9-methyl 7-(2,2,2-trichloroethyl) (6aR,9R,10aR)-6,6a,8,9,10,10a-hexahydroindolo[4,3-fg]quinoline-7,9(4H)-dicarboxylate
- 85329-86-8
(6aR,9R,10aR)-7-allyl-N-[3-(dimethylamino)propyl]-4,6,6a,7,8,9,10,10a-octahydroindolo[4,3-fg]quinoline-9-carboxamide
| Conditions | Yield |
|---|---|
| Multi-step reaction with 3 steps 1: zinc / methanol; acetic acid / 1.08 h / 20 °C 2: potassium carbonate / N,N-dimethyl-formamide / 2.5 h / 35 °C 3: acetic acid / 24 h / Reflux View Scheme |
- 30341-92-5
methyl (6aR,9R,10aR)-4,6,6a,7,8,9,10,10a-octahydroindolo[4,3-fg]quinoline-9-carboxylate
- 85329-86-8
(6aR,9R,10aR)-7-allyl-N-[3-(dimethylamino)propyl]-4,6,6a,7,8,9,10,10a-octahydroindolo[4,3-fg]quinoline-9-carboxamide
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1: potassium carbonate / N,N-dimethyl-formamide / 2.5 h / 35 °C 2: acetic acid / 24 h / Reflux View Scheme |
- 25447-66-9
Dihydroergocryptine
- 85329-86-8
(6aR,9R,10aR)-7-allyl-N-[3-(dimethylamino)propyl]-4,6,6a,7,8,9,10,10a-octahydroindolo[4,3-fg]quinoline-9-carboxamide
| Conditions | Yield |
|---|---|
| Multi-step reaction with 6 steps 1: sodium hydroxide; sodium dithionite / water / 4 h / Reflux 2: sulfuric acid / 15 h / 20 °C 3: dmap / dichloromethane / 16 h / Reflux; Inert atmosphere 4: zinc / methanol; acetic acid / 1.08 h / 20 °C 5: potassium carbonate / N,N-dimethyl-formamide / 2.5 h / 35 °C 6: acetic acid / 24 h / Reflux View Scheme |
- 5878-43-3
9,10-dihydrolysergic acid
- 85329-86-8
(6aR,9R,10aR)-7-allyl-N-[3-(dimethylamino)propyl]-4,6,6a,7,8,9,10,10a-octahydroindolo[4,3-fg]quinoline-9-carboxamide
| Conditions | Yield |
|---|---|
| Multi-step reaction with 5 steps 1: sulfuric acid / 15 h / 20 °C 2: dmap / dichloromethane / 16 h / Reflux; Inert atmosphere 3: zinc / methanol; acetic acid / 1.08 h / 20 °C 4: potassium carbonate / N,N-dimethyl-formamide / 2.5 h / 35 °C 5: acetic acid / 24 h / Reflux View Scheme |
- 24424-99-5
di-tert-butyl dicarbonate
- 85329-86-8
(6aR,9R,10aR)-7-allyl-N-[3-(dimethylamino)propyl]-4,6,6a,7,8,9,10,10a-octahydroindolo[4,3-fg]quinoline-9-carboxamide
- 474397-67-6
tert-butyl (5R,8R,10R)-6-allyl-8-[[[3-(dimethylamino)propyl]amino]carbonyl]ergoline-1-carboxylate
| Conditions | Yield |
|---|---|
| With dmap In tetrahydrofuran at 40℃; for 2h; | 92% |
- 18162-48-6
tert-butyldimethylsilyl chloride
- 85329-86-8
(6aR,9R,10aR)-7-allyl-N-[3-(dimethylamino)propyl]-4,6,6a,7,8,9,10,10a-octahydroindolo[4,3-fg]quinoline-9-carboxamide
| Conditions | Yield |
|---|---|
| Stage #1: (6aR,9R,10aR)-7-allyl-N-[3-(dimethylamino)propyl]-4,6,6a,7,8,9,10,10a-octahydroindolo[4,3-fg]quinoline-9-carboxamide With sodium hydride In tetrahydrofuran at 20℃; for 1.5h; Stage #2: tert-butyldimethylsilyl chloride In tetrahydrofuran at 20℃; for 1.25h; | 86.5% |
- 85329-86-8
(6aR,9R,10aR)-7-allyl-N-[3-(dimethylamino)propyl]-4,6,6a,7,8,9,10,10a-octahydroindolo[4,3-fg]quinoline-9-carboxamide
- 109-90-0
ethyl isocyanate
A
- 81409-90-7
cabergoline
B
- 126554-50-5
(6aR,9R,10aR)-7-allyl-N9-[3-(dimethylamino)propyl]-N4-ethyl-N9-(ethylcarbamoyl)-6a,7,8,9,10,10a-hexahydroindolo[4,3-fg]quinoline-4,9(6H)-dicarboxamide
| Conditions | Yield |
|---|---|
| In toluene Heating; | A 81% B 0.57 g |
- 85329-86-8
(6aR,9R,10aR)-7-allyl-N-[3-(dimethylamino)propyl]-4,6,6a,7,8,9,10,10a-octahydroindolo[4,3-fg]quinoline-9-carboxamide
- 624-83-9
methyl isocyanate
- 126554-48-1
N-<3-(dimethylamino)propyl>-N-<(methylamino)-carbonyl>-6-(2-propenyl)-ergoline-8β-carboxamide
| Conditions | Yield |
|---|---|
| 80% |
- Total:17 Page 1 of 1 1
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