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88023-83-0

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Basic Information
CAS No.: 88023-83-0
Name: Benzene, 1-methoxy-4-[[(methylthio)methoxy]methyl]-
Article Data: 9
Molecular Structure:
Molecular Structure of 88023-83-0 (Benzene, 1-methoxy-4-[[(methylthio)methoxy]methyl]-)
Formula: C10H14O2S
Molecular Weight: 198.286
Synonyms: 4-methoxybenzyl methylthiomethyl ether;p-methoxybenzyl methylthiomethyl ether;p-methoxybenzyloxymethyl methyl sulfide;4-methoxy-benzyloxymethyl methyl sulfide;
PSA: 43.76000
LogP: 2.53230
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Synthetic route
2373-51-5

chloro-methylsulfanyl-methane

105-13-5

4-Methoxybenzyl alcohol

88023-83-0

1-methoxy-4-{[(methylsulfanyl)methoxy]methyl}-benzene

Conditions
ConditionsYield
Stage #1: 4-Methoxybenzyl alcohol With sodium hydride; sodium iodide In tetrahydrofuran at 0 - 20℃; Inert atmosphere;
Stage #2: chloro-methylsulfanyl-methane In tetrahydrofuran at 0 - 20℃; for 12h;		95%
Stage #1: 4-Methoxybenzyl alcohol With sodium hydride; sodium iodide In tetrahydrofuran; mineral oil at 0 - 20℃; for 1h; Inert atmosphere;
Stage #2: chloro-methylsulfanyl-methane In tetrahydrofuran; mineral oil at 0 - 20℃; for 12h; Inert atmosphere;		95%
With sodium hydride; sodium iodide In tetrahydrofuran; mineral oil at 0 - 20℃; for 20h; Inert atmosphere;86%
75-18-3

dimethylsulfide

105-13-5

4-Methoxybenzyl alcohol

88023-83-0

1-methoxy-4-{[(methylsulfanyl)methoxy]methyl}-benzene

Conditions
ConditionsYield
With Perbenzoic acid In acetonitrile at 0℃; for 3h;81%
2373-51-5

chloro-methylsulfanyl-methane

53942-86-2

4-methoxybenzyl alcohol sodium salt

88023-83-0

1-methoxy-4-{[(methylsulfanyl)methoxy]methyl}-benzene

4779-31-1

Z-Asp-OBn

88023-83-0

1-methoxy-4-{[(methylsulfanyl)methoxy]methyl}-benzene

(S)-2-Benzyloxycarbonylamino-succinic acid 1-benzyl ester 4-(4-methoxy-benzyloxymethyl) ester

Conditions
ConditionsYield
With tetrabutylammomium bromide; copper(ll) bromide In N,N-dimethyl-formamide at 0℃; for 28h;100%
20806-43-3

Z-Ser(Bzl)-OH

88023-83-0

1-methoxy-4-{[(methylsulfanyl)methoxy]methyl}-benzene

(S)-3-Benzyloxy-2-benzyloxycarbonylamino-propionic acid 4-methoxy-benzyloxymethyl ester

Conditions
ConditionsYield
With tetrabutylammomium bromide; copper(ll) bromide In dichloromethane at 0℃; for 27h;100%
88023-83-0

1-methoxy-4-{[(methylsulfanyl)methoxy]methyl}-benzene

150-76-5

4-methoxy-phenol

C16H18O4

Conditions
ConditionsYield
With tetrabutylammomium bromide; copper(ll) bromide In dichloromethane at 0℃; for 5h;95%
88023-83-0

1-methoxy-4-{[(methylsulfanyl)methoxy]methyl}-benzene

4064-06-6

1,2:3,4-di-O-isopropylidene-α-D-galactopyranose

(3aR,5R,5aS,8aS,8bR)-5-(4-Methoxy-benzyloxymethoxymethyl)-2,2,7,7-tetramethyl-tetrahydro-bis[1,3]dioxolo[4,5-b;4',5'-d]pyran

Conditions
ConditionsYield
With tetrabutylammomium bromide; copper(ll) bromide In N,N-dimethyl-formamide at 20℃; for 1h; Product distribution; Further Variations:; Reaction partners; Solvents; Temperatures;92%
88023-83-0

1-methoxy-4-{[(methylsulfanyl)methoxy]methyl}-benzene

99-94-5

p-Toluic acid

4-methyl-benzoic acid 4-methoxy-benzyloxymethyl ester

Conditions
ConditionsYield
With tetrabutylammomium bromide; copper(ll) bromide In dichloromethane at 20℃; for 4h;88%
25018-67-1

1,2;4,5-di-O-isopropylidene-β-D-(-)-fructopyranose

88023-83-0

1-methoxy-4-{[(methylsulfanyl)methoxy]methyl}-benzene

C21H30O8

Conditions
ConditionsYield
With tetrabutylammomium bromide; copper(ll) bromide In 1,2-dichloro-ethane; N,N-dimethyl-formamide at 20℃; for 2h;84%
88023-83-0

1-methoxy-4-{[(methylsulfanyl)methoxy]methyl}-benzene

88023-78-3

para-methoxybenzyl chloride

Conditions
ConditionsYield
With acetyl chloride In dichloromethane Inert atmosphere;80%
With sulfuryl dichloride In dichloromethane at -78℃; for 0.5h;70%
With sulfuryl dichloride In dichloromethane at -78℃;
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    Benzene, 1-methoxy-4-[[(methylthio)methoxy]methyl]-

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  • 4-methoxybenzyl methylthiomethyl ether

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    4-methoxybenzyl methylthiomethyl ether

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