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89996-00-9

Basic Information
CAS No.: 89996-00-9
Name: Phosphonium, (2-aminoethyl)triphenyl-, bromide
Article Data: 13
Molecular Structure:
Molecular Structure of 89996-00-9 (Phosphonium, (2-aminoethyl)triphenyl-, bromide)
Formula: C20H21NP.Br
Molecular Weight: 467.183
PSA: 39.61000
LogP: 0.64350
Synthetic route
107-09-5

2-bromoethylamine

603-35-0

triphenylphosphine

89996-00-9

(2-aminoethyl)triphenylphosphonium bromide salt

Conditions
ConditionsYield
In acetonitrile for 24h; Reflux;88%
2576-47-8

2-bromoethylamine hydrobromide

603-35-0

triphenylphosphine

89996-00-9

(2-aminoethyl)triphenylphosphonium bromide salt

Conditions
ConditionsYield
In acetonitrile for 18h; Reflux;68%
In acetonitrile for 15h; Reflux; Inert atmosphere;40%
In acetonitrile for 15h; Heating;19%

satraplatin

89996-00-9

(2-aminoethyl)triphenylphosphonium bromide salt

C41H64Cl2N4O5PPt(1+)*Cl(1-)

Conditions
ConditionsYield
Stage #1: satraplatin With HATU In N,N-dimethyl-formamide for 0.333333h;
Stage #2: (2-aminoethyl)triphenylphosphonium bromide salt In N,N-dimethyl-formamide at 20℃; for 0.5h;
Stage #3: With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 5.5h;
94%

5-amino-1-naphthalenesulfonyl chloride

89996-00-9

(2-aminoethyl)triphenylphosphonium bromide salt

C30H28N2O2PS(1+)

Conditions
ConditionsYield
Stage #1: (2-aminoethyl)triphenylphosphonium bromide salt With triethylamine In dichloromethane at 20℃; for 0.25h;
Stage #2: 5-amino-1-naphthalenesulfonyl chloride In dichloromethane
94%

cyclohexa-2,4-dien-1-ylmethyl (2,5-dioxopyrrolidin-1-yl) carbonate

89996-00-9

(2-aminoethyl)triphenylphosphonium bromide salt

(2-(((cyclohexa-2,4-dien-1-ylmethoxy)carbonyl)amino)ethyl)triphenylphosphonium bromide

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In acetonitrile at 20℃; for 4h;91%

2,5-dioxopyrrolidin-1-yl ((1,2,3,4,5-pentamethylcyclopenta-2,4-dien-1-yl)methyl) carbonate

89996-00-9

(2-aminoethyl)triphenylphosphonium bromide salt

(2-((((1,2,3,4,5-pentamethylcyclopenta-2,4-dien-1-yl)methoxy)carbonyl)amino)ethyl)triphenylphosphonium bromide

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In acetonitrile at 20℃; for 4h;87%

(4R*,5R*)-5-diisopropyloxyphosphoryl-5-methyl-4-(succinimidyloxycarbonyloxymethyl)-1-pyrroline N-oxide

89996-00-9

(2-aminoethyl)triphenylphosphonium bromide salt

(4R*,5R*)-5-(diisopropyloxyphosphoryl)-5-methyl-4-[({[2-(triphenylphosphonio)ethyl]carbamoyl}oxy)methyl]pyrroline N-oxide bromide

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃; for 3h; Inert atmosphere;86%
53293-00-8

hex-5-ynoic acid

89996-00-9

(2-aminoethyl)triphenylphosphonium bromide salt

(2-(hex-5-ynamido)ethyl)triphenylphosphonium bromide

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine; HATU In N,N-dimethyl-formamide at 20℃; for 24h;84%

((2-(2-(fluoro-18F)ethoxy)ethyl)sulfonyl)ethane

89996-00-9

(2-aminoethyl)triphenylphosphonium bromide salt

C26H32(18)FNO3PS(1+)*Br(1-)

Conditions
ConditionsYield
at 45 - 65℃; pH=8.5;81%
13574-13-5

Boc-Glu(OBzl)-OH

89996-00-9

(2-aminoethyl)triphenylphosphonium bromide salt

C37H42N2O5P(1+)*Br(1-)

Conditions
ConditionsYield
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 16h;76%
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