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CAS No.: | 89996-00-9 |
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Name: | Phosphonium, (2-aminoethyl)triphenyl-, bromide |
Article Data: | 13 |
Molecular Structure: | |
Formula: | C20H21NP.Br |
Molecular Weight: | 467.183 |
PSA: | 39.61000 |
LogP: | 0.64350 |
2-bromoethylamine
triphenylphosphine
(2-aminoethyl)triphenylphosphonium bromide salt
Conditions | Yield |
---|---|
In acetonitrile for 24h; Reflux; | 88% |
2-bromoethylamine hydrobromide
triphenylphosphine
(2-aminoethyl)triphenylphosphonium bromide salt
Conditions | Yield |
---|---|
In acetonitrile for 18h; Reflux; | 68% |
In acetonitrile for 15h; Reflux; Inert atmosphere; | 40% |
In acetonitrile for 15h; Heating; | 19% |
Conditions | Yield |
---|---|
Stage #1: satraplatin With HATU In N,N-dimethyl-formamide for 0.333333h; Stage #2: (2-aminoethyl)triphenylphosphonium bromide salt In N,N-dimethyl-formamide at 20℃; for 0.5h; Stage #3: With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 5.5h; | 94% |
(2-aminoethyl)triphenylphosphonium bromide salt
Conditions | Yield |
---|---|
Stage #1: (2-aminoethyl)triphenylphosphonium bromide salt With triethylamine In dichloromethane at 20℃; for 0.25h; Stage #2: 5-amino-1-naphthalenesulfonyl chloride In dichloromethane | 94% |
(2-aminoethyl)triphenylphosphonium bromide salt
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In acetonitrile at 20℃; for 4h; | 91% |
(2-aminoethyl)triphenylphosphonium bromide salt
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In acetonitrile at 20℃; for 4h; | 87% |
(2-aminoethyl)triphenylphosphonium bromide salt
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 3h; Inert atmosphere; | 86% |
hex-5-ynoic acid
(2-aminoethyl)triphenylphosphonium bromide salt
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; HATU In N,N-dimethyl-formamide at 20℃; for 24h; | 84% |
(2-aminoethyl)triphenylphosphonium bromide salt
Conditions | Yield |
---|---|
at 45 - 65℃; pH=8.5; | 81% |
Boc-Glu(OBzl)-OH
(2-aminoethyl)triphenylphosphonium bromide salt
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 16h; | 76% |