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Cas Database |
| Name |
2-(Methylthio)acetamide |
EINECS | N/A |
| CAS No. | 22551-24-2 | Density | 1.132 g/cm3 |
| PSA | 68.39000 | LogP | 0.53500 |
| Solubility | N/A | Melting Point |
99-102 °C |
| Formula | C3H7NOS | Boiling Point | 258.8 °C at 760 mmHg |
| Molecular Weight | 105.161 | Flash Point | 110.3 °C |
| Transport Information | N/A | Appearance | white solid |
| Safety | Risk Codes | N/A | |
| Molecular Structure |
|
Hazard Symbols | N/A |
| Synonyms |
(Methylthio)acetamide; |
Article Data | 8 |
2-(Methylthio)acetamide Synthetic route
- 35928-65-5
(methylthio)acetyl chloride
- 22551-24-2
2-(methylthio)acetamide
| Conditions | Yield |
|---|---|
| With ammonia In diethyl ether at 0℃; | 97% |
| With ammonia In benzene for 0.0833333h; |
- 16630-66-3
methyl 2-(methylthio)acetate
- 22551-24-2
2-(methylthio)acetamide
| Conditions | Yield |
|---|---|
| With ammonium hydroxide at 20 - 25℃; for 2.25h; | 76.2% |
- 4455-13-4
methylthioacetic acid ethyl ester
- 22551-24-2
2-(methylthio)acetamide
| Conditions | Yield |
|---|---|
| With ammonia |
| Conditions | Yield |
|---|---|
| With ethanol |
- 35120-10-6
methylthioacetonitrile
A
- 22551-24-2
2-(methylthio)acetamide
B
- 2444-37-3
methylsulfanyl-acetic acid
| Conditions | Yield |
|---|---|
| With potassium phosphate buffer; lyophilized Zea mays nitrilase ZmNIT2 EC 3.5.5.1 In water at 30℃; for 14h; pH=7.15; Title compound not separated from byproducts; |
| Conditions | Yield |
|---|---|
| Stage #1: methyl chloroacetate; sodium thiomethoxide With tetramethylammonium bromide at 20 - 50℃; for 1h; Stage #2: With ammonium hydroxide at 0 - 5℃; | 55.85 g |
- 4784-77-4, 39616-19-8, 29576-14-5
(E)-1-Bromo-2-butene
- 22551-24-2
2-(methylthio)acetamide
- 343269-10-3
3-Methyl-2-methylsulfanyl-pent-4-enoic acid amide
| Conditions | Yield |
|---|---|
| With potassium carbonate for 48h; | 95% |
- 22551-24-2
2-(methylthio)acetamide
- 37677-17-1
1-bromomethylcyclohexene
- 72730-26-8
2-(2-Methylene-cyclohexyl)-2-methylsulfanyl-acetamide
| Conditions | Yield |
|---|---|
| With potassium carbonate for 48h; | 92% |
- 22551-24-2
2-(methylthio)acetamide
- 81442-38-8
α-(Methylsulfinyl)-acetamide
| Conditions | Yield |
|---|---|
| With NaJO4 In methanol; water Ambient temperature; overnight; | 90% |
| With dihydrogen peroxide; acetone |
- 22551-24-2
2-(methylthio)acetamide
- 2835-77-0
(2-aminophenyl)(phenyl)methanone
- 78281-61-5
2-amino-3-benzoyl-α-(methylthio)benzeneacetamide
| Conditions | Yield |
|---|---|
| Stage #1: 2-(methylthio)acetamide; (2-aminophenyl)(phenyl)methanone With N-chloro-succinimide In dichloromethane at -45 - 8℃; Stage #2: With triethylamine In dichloromethane Product distribution / selectivity; | 86.4% |
| Stage #1: (2-aminophenyl)(phenyl)methanone With N-chloro-succinimide In dichloromethane at -35 - -25℃; for 0.5h; Stage #2: 2-(methylthio)acetamide In dichloromethane at 0 - 10℃; for 2h; Solvent; | 80.27% |
| Stage #1: 2-(methylthio)acetamide; (2-aminophenyl)(phenyl)methanone With N-chlorophthalimide In dichloromethane at -20 - -5℃; for 3.5h; Stage #2: With triethylamine In dichloromethane Stage #3: With potassium hydroxide In dichloromethane; water Temperature; Concentration; | 63.1% |
2-(Methylthio)acetamide Specification
The 2-(Methylthio)acetamide ,its cas register number is 22551-24-2.It also can be called as Acetamide,2-(methylthio)- and the Systematic name about this chemicals is 2-(Methylsulfanyl)acetamide .It is a white solid and can be used as Pharmaceutical Intermediates.If you want to sotre this chemicals, please keep containers tightly sealed, and store in cool, dry place in tighely closed containers.
Following are the chemical properties about 2-(Methylthio)acetamide : (1)#H bond acceptors: 2 ; (2)#H bond donors: 2 ; (3)#Freely Rotating Bonds: 2 ; (4)Polar Surface Area: 45.61 Å ; (5)Index of Refraction: 1.504 ; (6)Molar Refractivity: 27.5 cm3 ; (7)Molar Volume: 92.8 cm3 ; (8)Surface Tension: 41.9 dyne/cm; (9)Enthalpy of Vaporization: 49.64 kJ/mol ; (10)Vapour Pressure: 0.0135 mmHg at 25°C .
This chemicals can be described computed from structure:
(1)SMILES: O=C(N)CSC
(2)InChI: InChI=1/C3H7NOS/c1-6-2-3(4)5/h2H2,1H3,(H2,4,5)
(3)InChIKey: OBENGAMZEGRSIC-UHFFFAOYAN
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