2,3-Decanedione

Base Information

• Chemical Name: 2,3-Decanedione
• CAS No.: 3848-26-8
• Molecular Formula: C10H18O2
• Molecular Weight: 170.252
• Hs Code.: 2914190090
• Mol file: 3848-26-8.mol

Synonyms:decan-8,9-dione;2,3-Decanedione;

Chemical Property of 2,3-Decanedione

Chemical Property:

• PSA: 34.14000
• LogP: 2.50500

Purity/Quality:

99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,3-Decanedione

There total 14 articles about 2,3-Decanedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

trans-3,4-epoxydecan-2-one (420849-80-5) → decane-2,3-dione (3848-26-8)

Guidance literature:

{iron(III) tetraphenylporphyrin}triflate; In 1,4-dioxane; for 1.5h; Heating;

DOI:10.1039/b207328e

Reference yield: 90.1%

2,3-didecanol → decane-2,3-dione (3848-26-8)

Guidance literature:

With 4-acetylamino-2,2,6,6-tetramethyl-1-piperidinoxy; In 1,2-dichloro-ethane; at 40 ℃; for 4h; Inert atmosphere;

Reference yield: 89.0%

2,3-dichlorodecene-2 → decane-2,3-dione (3848-26-8) + valeric acid (109-52-4)

Guidance literature:

With ruthenium(IV) oxide; sodium periodate; In dichloromethane; water; acetonitrile; for 0.25h; Ambient temperature;

DOI:10.1080/00397919508011819

upstream raw materials:

3,4-epoxy-2-decanone

2-Methoxy-dec-1-en-3-one

trans-3,4-epoxydecan-2-one

Decan-2-one

Refernces

• 1、 Rüedi, Georg,Oberli, Matthias A.,Nagel, Matthias,Weymuth, Christophe,Hansen, Hans-Jürgen. "A practical and user-friendly method for the selenium-free one-step preparation of 1,2-diketones and their monoxime analogs". . p. 2315 - 2318. Retrieved 2007/10/03.
• 2、 -. "SUBSTITUTED FUSED AND BRIDGED BICYCLIC COMPOUNDS AS THERAPEUTIC AGENTS". . . Retrieved 2008/06/13.