Tricyclohexylmethane.

Base Information

• Chemical Name: Tricyclohexylmethane.
• CAS No.: 1610-24-8
• Molecular Formula: C19H34
• Molecular Weight: 262.479
• Hs Code.: 2902199090
• Mol file: 1610-24-8.mol

Synonyms:Methane,tricyclohexyl- (6CI,7CI,8CI); NSC 129189; Tricyclohexylmethane

Chemical Property of Tricyclohexylmethane.

Chemical Property:

• Melting Point: 48°C
• Refractive Index: 1.4986
• Boiling Point: 340.72°C (rough estimate)
• Flash Point: 158.3oC
• PSA: 0.00000
• Density: 0.9273
• LogP: 6.34350

Purity/Quality:

99%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Tricyclohexylmethane.

There total 21 articles about Tricyclohexylmethane. which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

triphenylmethane (519-73-3) → tricyclohexylmethane (1610-24-8)

Guidance literature:

With hydrogen; acetic acid; palladium on activated charcoal; In cyclohexane; at 170 ℃; for 22h; under 36200.4 Torr;

DOI:10.1021/jo00077a021

Reference yield: 90.0%

α,α-dicyclohexyl-cyclohexanemethanol (17687-74-0) → tricyclohexylmethane (1610-24-8)

Guidance literature:

With triethylsilane; trifluoroacetic acid; In dichloromethane; for 24h; Ambient temperature;

DOI:10.1021/jo00077a021

Reference yield: 87.0%

trifluoro-acetic acid tricyclohexylmethyl ester → tricyclohexylmethane (1610-24-8)

Guidance literature:

With diphenylsilane; at 130 ℃; for 15h;

DOI:10.1016/j.tetlet.2004.02.109

upstream raw materials:

triphenylmethyl alcohol

triphenylmethane

tetraphenylmethane

4-benzhydrylphenol

Downstream raw materials:

tert-butylbenzene

triphenylmethane

dicyclohexyl-phenyl-methane

(cyclohexylmethylene)dibenzene

Refernces

• 1、 Gillies, D. G.,Luff, S.,Smith, G. W.,Sutcliffe, L. H.. "The structure of tricyclohexylmethane". . p. 113 - 122. Retrieved 1994.
• 2、 Kim, Joong-Gon,Cho, Dae Hyan,Jang, Doo Ok. "Radical deoxygenation of tertiary alcohols via trifluoroacetates". . p. 3031 - 3033. Retrieved 2007/10/03.