2-Benzhydrylideneoxolane

Base Information Edit

Chemical Name:2-Benzhydrylideneoxolane
CAS No.:39077-35-5
Molecular Formula:C17H16O
Molecular Weight:236.3083
Hs Code.:
NSC Number:101025
DSSTox Substance ID:DTXSID80295295
Wikidata:Q82035146
ChEMBL ID:CHEMBL1866354
Mol file:39077-35-5.mol

Synonyms:39077-35-5;MLS002703584;2-benzhydrylideneoxolane;NSC101025;NCIOpen2_006846;CHEMBL1866354;DTXSID80295295;NSC-101025;SMR001570301

Suppliers and Price of 2-Benzhydrylideneoxolane

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 2-Benzhydrylideneoxolane Edit

Chemical Property:

Vapor Pressure:2.19E-05mmHg at 25°C
Boiling Point:371.5°Cat760mmHg
Flash Point:176.1°C
Density:1.104g/cm³
XLogP3:4.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:236.120115130
Heavy Atom Count:18
Complexity:273

Purity/Quality:: 99%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC(=C(C2=CC=CC=C2)C3=CC=CC=C3)OC1

Technology Process of 2-Benzhydrylideneoxolane

There total 4 articles about 2-Benzhydrylideneoxolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 4545-20-4
benzophenone tosylhydrazone

: 927-74-2
3-Butyn-1-ol

: 39077-35-5
2-(diphenylmethylene)tetrahydrofuran

Guidance literature:: benzophenone tosylhydrazone; 3-Butyn-1-ol; With copper(l) iodide; bathophenanthroline; tetrabutylammomium bromide; lithium tert-butoxide; In 1,4-dioxane; at 110 ℃; for 4h; Inert atmosphere;

With toluene-4-sulfonic acid; at 80 ℃; for 2h; Reagent/catalyst; Inert atmosphere;
DOI:10.1016/S1872-2067(16)62565-2

Reference yield: 40.0%

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 119-61-9
benzophenone

: 39077-35-5
2-(diphenylmethylene)tetrahydrofuran

Guidance literature:: tetrahydrofuran; benzophenone; In neat (no solvent); at 60 ℃; for 12h; UV-irradiation; Inert atmosphere;

With trifluoroacetic acid; trifluoroacetic anhydride; at 60 ℃; for 3h;
DOI:10.1039/c6cc07626b