Benzene-1,3,5-tricarbohydrazide

Base Information

• Chemical Name: Benzene-1,3,5-tricarbohydrazide
• CAS No.: 36997-31-6
• Molecular Formula: C9H12N6O3
• Molecular Weight: 252.233
• DSSTox Substance ID: DTXSID801252329
• Nikkaji Number: J3.478.466C
• Mol file: 36997-31-6.mol

Synonyms:Benzene-1,3,5-tricarbohydrazide;36997-31-6;Benzene-1,3,5-tricarboxylic acid trihydrazide;Trimesinsaure-trihydrazid;YSZC213;SCHEMBL1893743;DTXSID801252329;MFCD16172194;BS-44802;Benzene-1,3,5-tricarboxylicacidtrihydrazide;CS-0111292;1,3,5-Benzenetricarboxylic acid, trihydrazide;D80785

Chemical Property of Benzene-1,3,5-tricarbohydrazide

Chemical Property:

• XLogP3: -2.5
• Hydrogen Bond Donor Count: 6
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 3
• Exact Mass: 252.09708827
• Heavy Atom Count: 18
• Complexity: 283

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1=C(C=C(C=C1C(=O)NN)C(=O)NN)C(=O)NN

Technology Process of Benzene-1,3,5-tricarbohydrazide

There total 4 articles about Benzene-1,3,5-tricarbohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

1,3,5-tris-(methoxycarbonyl)benzene (2672-58-4) → benzene-1,3,5-tricarboxylic acid trihydrazide (36997-31-6)

Guidance literature:

With hydrazine hydrate; In ethanol; toluene; at 110 ℃; for 24h; Inert atmosphere;

DOI:10.1021/jp9093063

Reference yield:

triethyl benzene-1,3,5-tricarboxylate (4105-92-4) → benzene-1,3,5-tricarboxylic acid trihydrazide (36997-31-6)

Guidance literature:

With ethanol; hydrazine hydrate;

Reference yield:

1,3,5-benzene tris(carbonyl chloride) (4422-95-1) → benzene-1,3,5-tricarboxylic acid trihydrazide (36997-31-6)

Guidance literature:

With hydrazine hydrate;

upstream raw materials:

triethyl benzene-1,3,5-tricarboxylate

1,3,5-benzene tris(carbonyl chloride)

benzene-1,3,5-tricarboxylic acid

1,3,5-tris-(methoxycarbonyl)benzene

Downstream raw materials:

benzene-1,3,5-tricarboxylic acid tris-(N'-benzenesulfonyl-hydrazide)

Benzene-1,3,5-tricarboxylic acid tris(2-benzoyl>hydrazide)

1,3,5-benzenetricarbonyl triazide

Refernces

• 1、 He, Cheng,Lin, Zhihua,He, Zheng,Duan, Chunying,Xu, Chunhu,Wang, Zheming,Yan, Chunhua. "Metal-tunable nanocages as artificial chemosensors". . p. 877 - 881. Retrieved 2008.
• 2、 Chen, Jian-Jun,Cui, Tian-Lu,Wang, Hui,Zhang, Bo-Wen,Zhang, Wen-Bei,Zhang, Xue-Jing. "Fabrication of conjugated polyimides with porous crosslinked networks and their application as cathodes for lithium-ion batteries". supporting information. p. 18764 - 18768. Retrieved 2021/10/29.
• 3、 -. "Organogel compound with AIE effect as well as preparation method and application of organogel compound". Paragraph 0031-0032. . Retrieved 2021/01/04.