Technology Process of 2-Methoxybenzenethiol
There total 32 articles about 2-Methoxybenzenethiol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper(ll) sulfate pentahydrate; ethane-1,2-dithiol; potassium hydroxide;
In
water; dimethyl sulfoxide;
at 90 ℃;
for 20h;
Inert atmosphere;
DOI:10.1002/adsc.201400941
- Guidance literature:
-
With
N,N,N,N,N,N-hexamethylphosphoric triamide; sodium hydride; diethylamine;
In
xylene;
for 6h;
Heating;
DOI:10.1055/s-1982-29868
- Guidance literature:
-
2-bromoanisole;
With
water; caesium carbonate; sodium thiosulfate; bis(dibenzylideneacetone)-palladium(0); XPhos;
In
toluene; tert-butyl alcohol;
at 80 ℃;
for 24h;
Inert atmosphere;
With
hydrogenchloride; zinc;
In
water;
for 1h;
Cooling with ice;
DOI:10.1016/j.tetlet.2010.10.128
Xn,
Xi
