Tricyclo[4.3.1.13,8]undecan-1-amine

Base Information

• Chemical Name: Tricyclo[4.3.1.13,8]undecan-1-amine
• CAS No.: 31083-61-1
• Molecular Formula: C11H19N
• Molecular Weight: 165.28
• Hs Code.: 2921300090
• Mol file: 31083-61-1.mol

Synonyms:Tricyclo[4.3.1.13,8]undecan-1-amine

Chemical Property of Tricyclo[4.3.1.13,8]undecan-1-amine

Chemical Property:

• Boiling Point: 245.6±8.0 °C(Predicted)
• PKA: 10.76±0.20(Predicted)
• PSA: 26.02000
• Density: 1.036±0.06 g/cm3(Predicted)
• LogP: 3.00430

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Tricyclo[4.3.1.13,8]undecan-1-amine

There total 5 articles about Tricyclo[4.3.1.13,8]undecan-1-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Homoadamantane-1-carboxylic acid (31061-65-1) → 1-Amino-homoadamantan (31083-61-1)

Guidance literature:

Multi-step reaction with 2 steps

1: HgO, Br₂ / CCl₄

2: (i) H₂SO₄, (ii) NaOH

With bromine; mercury(II) oxide; In tetrachloromethane;

DOI:10.1007/BF00853388

Reference yield:

3-Hydroxyhomoadamantan (14504-80-4) → 1-Amino-homoadamantan (31083-61-1)

Guidance literature:

Multi-step reaction with 3 steps

1: H₂SO₄

2: HgO, Br₂ / CCl₄

3: (i) H₂SO₄, (ii) NaOH

With sulfuric acid; bromine; mercury(II) oxide; In tetrachloromethane;

DOI:10.1007/BF00853388

Reference yield:

3-Acetamido-homoadamantan (27011-43-4) → 1-Amino-homoadamantan (31083-61-1)

Guidance literature:

Multi-step reaction with 4 steps

1: aq. HCl

2: H₂SO₄

3: HgO, Br₂ / CCl₄

4: (i) H₂SO₄, (ii) NaOH

With hydrogenchloride; sulfuric acid; bromine; mercury(II) oxide; In tetrachloromethane;

DOI:10.1007/BF00853388

upstream raw materials:

1-Brom-homoadamantan

acetonitrile

Homoadamantane-1-carboxylic acid

3-Hydroxyhomoadamantan

Downstream raw materials:

Homoadamantan-1-ol

3-Hydroxyhomoadamantan