1-Bromo-4-dibenzofuranamine

Base Information Edit

Chemical Name:1-Bromo-4-dibenzofuranamine
CAS No.:50548-39-5
Molecular Formula:C12H8BrNO
Molecular Weight:262.106
Hs Code.:
Mol file:50548-39-5.mol

Synonyms:1-Bromo-4-aminodibenzofuran;1-Bromo-4-dibenzofuranamine;1-broModibenzo[b,d]furan-4-aMine;1-bromo-dibenzofuran-4-ylamine;1-Brom-4-aminodibenzofuran

Suppliers and Price of 1-Bromo-4-dibenzofuranamine

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 17 raw suppliers

Chemical Property of 1-Bromo-4-dibenzofuranamine Edit

Chemical Property:

Melting Point:119-120℃
PSA：39.16000
LogP:4.51190

Purity/Quality:: 99.3% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-Bromo-4-dibenzofuranamine

There total 6 articles about 1-Bromo-4-dibenzofuranamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 50548-38-4
1-bromo-N-(4-dibenzofuranyl)acetamide

: 50548-39-5
1-bromodibenzo[b,d]furan-1-amine

Guidance literature:: With potassium hydroxide; In tetrahydrofuran; ethanol; water; Reflux;

Reference yield:

: 50548-37-3
N-(4-dibenzofuranyl)acetamide

: 50548-39-5
1-bromodibenzo[b,d]furan-1-amine

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid; bromine

2: ethanolic KOH-solution

With potassium hydroxide; bromine; acetic acid;
DOI:10.1021/ja01875a013

Reference yield:

: 89827-45-2
4-bromodibenzofuran

: 50548-39-5
1-bromodibenzo[b,d]furan-1-amine

Guidance literature:: Multi-step reaction with 3 steps

1.1: (1R,2R)-1,2-diaminocyclohexane; copper(l) iodide; potassium carbonate / toluene / Reflux

2.1: bromine; acetic acid / 4 h / 20 °C

2.2: Reflux

3.1: potassium hydroxide / tetrahydrofuran; water; ethanol / 4 h / 20 °C / Reflux

With copper(l) iodide; (1R,2R)-1,2-diaminocyclohexane; bromine; potassium carbonate; acetic acid; potassium hydroxide; In tetrahydrofuran; ethanol; water; toluene;