Technology Process of 1-(2-Isocyanophenyl)pyrrole
There total 3 articles about 1-(2-Isocyanophenyl)pyrrole which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
triethylamine; trichlorophosphate;
In
tetrahydrofuran;
at 0 ℃;
DOI:10.1246/cl.1998.551
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 70 percent / 216 h / Heating
2: 78 percent / triethylamine; phosphoryl chloride / tetrahydrofuran / 0.2 h / 0 °C
With
triethylamine; trichlorophosphate;
In
tetrahydrofuran;
DOI:10.1246/bcsj.74.1109
- Guidance literature:
-
Multi-step reaction with 3 steps
1: copper(l) iodide; potassium phosphate; N,N-dimethylethylenediamine / toluene / 24 h / 110 °C / Inert atmosphere
2: tetrahydrofuran / 0.5 h / 0 - 20 °C
3: trichlorophosphate; triethylamine / tetrahydrofuran / 4 h / 0 °C
With
potassium phosphate; copper(l) iodide; N,N-dimethylethylenediamine; triethylamine; trichlorophosphate;
In
tetrahydrofuran; toluene;
DOI:10.1021/acs.orglett.7b00375
