CHEMBRDG-BB 4009817

Base Information

• Chemical Name: CHEMBRDG-BB 4009817
• CAS No.: 1859-37-6
• Molecular Formula: C13H20N2
• Molecular Weight: 204.315
• Hs Code.: 2933399090
• Mol file: 1859-37-6.mol

Synonyms:TIMTEC-BB SBB005696;CHEMBRDG-BB 4009817;1-(1-METHYL-4-PHENYLPIPERIDIN-4-YL)METHANAMINE;1-(1-methyl-4-phenylpiperidin-4-yl)methanamine(SALTDATA: FREE);(1-methyl-4-phenyl-4-piperidinyl)methanamine;(1-methyl-4-phenyl-4-piperidyl)methanamine;(1-methyl-4-phenyl-4-piperidyl)methylamine;(1-methyl-4-phenyl-piperidin-4-yl)methanamine

Chemical Property of CHEMBRDG-BB 4009817

Chemical Property:

• Vapor Pressure: 0.000837mmHg at 25°C
• Boiling Point: 305.1°C at 760 mmHg
• PKA: 10.13±0.29(Predicted)
• Flash Point: 127.3°C
• PSA: 29.26000
• Density: 0.997g/cm³
• LogP: 2.24690

Purity/Quality:

98%,99%, ^*data from raw suppliers

1-(1-Methyl-4-phenylpiperidin-4-yl)methanamine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of CHEMBRDG-BB 4009817

There total 7 articles about CHEMBRDG-BB 4009817 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

1-methyl-4-phenyl-piperidine-4-carbonitrile (3627-62-1) → C-(1-methyl-4-phenyl-piperidin-4-yl)-methylamine (1859-37-6)

Guidance literature:

1-methyl-4-phenyl-piperidine-4-carbonitrile; With lithium aluminium tetrahydride; In tetrahydrofuran; for 2h;

With water; sodium sulfate; In tetrahydrofuran; for 0.5h;

Reference yield: 94.0%

→ C-(1-methyl-4-phenyl-piperidin-4-yl)-methylamine (1859-37-6)

Guidance literature:

Reference yield:

1-methyl-4-phenyl-piperidine-4-carbonitrile (3627-62-1) → C-(1-methyl-4-phenyl-piperidin-4-yl)-methylamine (1859-37-6) + (1-methyl-4-phenyl-[4]piperidylmethyl)-(1-methyl-4-phenyl-[4]piperidylmethylen)-amine (96074-20-3)

Guidance literature:

With nickel; at 100 ℃; under 66195.7 Torr; Hydrogenation;

upstream raw materials:

1-methyl-4-phenyl-piperidine-4-carbonitrile

diethyl ether

1-benzyl-4-phenyl-piperidine-4-carbonitrile; hydrochloride

4-phenyl-4-cyanopiperidine

Downstream raw materials:

C₂₈H₃₆N₆O

bis-(1-methyl-4-phenyl-[4]piperidylmethyl)-amine

methyl-(1-methyl-4-phenyl-piperidin-4-ylmethyl)-amine

N-(1-methyl-4-phenyl-[4]piperidylmethyl)-glycine-dimethylamide

Refernces

• 1、 -. "Duraglutin artificial antigen and preparation method thereof". Paragraph 0032; 0034. . Retrieved 2020/07/28.
• 2、 -. "NAPHTHAMIDE DERIVATIVES AND THEIR USE". Page 40; 44-45. . Retrieved 2010/02/06.