Technology Process of p-<(E)-2-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthyl)-propenyl>-benzoic acid isopropyl ester
There total 10 articles about p-<(E)-2-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthyl)-propenyl>-benzoic acid isopropyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridine;
In
diethyl ether;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: thionyl chloride, pyridine / N,N-dimethylformamide / diethyl ether
2: 85.3 percent / pyridine / diethyl ether / Ambient temperature
With
pyridine; thionyl chloride;
N,N-dimethyl-formamide;
In
diethyl ether;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 86 percent / potassium hydroxide / H2O; ethanol / 3 h / 50 °C
2: thionyl chloride, pyridine / N,N-dimethylformamide / diethyl ether
3: 85.3 percent / pyridine / diethyl ether / Ambient temperature
With
pyridine; potassium hydroxide; thionyl chloride;
N,N-dimethyl-formamide;
In
diethyl ether; ethanol; water;
