Technology Process of (3-hydroxy-5-iodophenyl) 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside
There total 4 articles about (3-hydroxy-5-iodophenyl) 2,3,4,6-tetra-O-acetyl-β-D-glucopyranoside which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: boron tribromide / dichloromethane / 12 h / -20 - 25 °C
2: silver carbonate / acetonitrile / 8 h / 25 °C
With
boron tribromide; silver carbonate;
In
dichloromethane; acetonitrile;
DOI:10.1515/znb-2011-0314
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydrogenchloride; sodium nitrite / water / 0 °C
1.2: 12 h / 0 - 25 °C
2.1: boron tribromide / dichloromethane / 12 h / -20 - 25 °C
3.1: silver carbonate / acetonitrile / 8 h / 25 °C
With
hydrogenchloride; boron tribromide; silver carbonate; sodium nitrite;
In
dichloromethane; water; acetonitrile;
DOI:10.1515/znb-2011-0314