Technology Process of 9-Deoxyclavulanic acid
There total 6 articles about 9-Deoxyclavulanic acid which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 70 percent / sodium hydroxide / H2O / 1.17 h / 0 °C
2: 69 percent / dimethylformamide / 1.5 h / Ambient temperature
3: 45 percent / H2 / palladium on carbon / tetrahydrofuran / 2.5 h / 735.5 Torr / Ambient temperature
4: 70 percent / dimethylformamide / 2 h / Ambient temperature
5: H2 / palladium on carbon / tetrahydrofuran
With
sodium hydroxide; hydrogen;
palladium on activated charcoal;
In
tetrahydrofuran; water; N,N-dimethyl-formamide;
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
tetrahydrofuran;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 69 percent / dimethylformamide / 1.5 h / Ambient temperature
2: 45 percent / H2 / palladium on carbon / tetrahydrofuran / 2.5 h / 735.5 Torr / Ambient temperature
3: 70 percent / dimethylformamide / 2 h / Ambient temperature
4: H2 / palladium on carbon / tetrahydrofuran
With
hydrogen;
palladium on activated charcoal;
In
tetrahydrofuran; N,N-dimethyl-formamide;
