Technology Process of sodium deoxyclavulanate
There total 1 articles about sodium deoxyclavulanate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 70 percent / sodium hydroxide / H2O / 1.17 h / 0 °C
2: 69 percent / dimethylformamide / 1.5 h / Ambient temperature
3: 45 percent / H2 / palladium on carbon / tetrahydrofuran / 2.5 h / 735.5 Torr / Ambient temperature
With
sodium hydroxide; hydrogen;
palladium on activated charcoal;
In
tetrahydrofuran; water; N,N-dimethyl-formamide;
- Guidance literature:
-
In
N,N-dimethyl-formamide;
for 2h;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 70 percent / dimethylformamide / 2 h / Ambient temperature
2: H2 / palladium on carbon / tetrahydrofuran
3: 50 percent / dicyclohexylcarbodi-imide / tetrahydrofuran / 4 h / Ambient temperature
With
hydrogen; dicyclohexyl-carbodiimide;
palladium on activated charcoal;
In
tetrahydrofuran; N,N-dimethyl-formamide;
