(2Z)-3-(2-methylphenyl)propenoic acid

Base Information Edit

Chemical Name:(2Z)-3-(2-methylphenyl)propenoic acid
CAS No.:41397-71-1
Molecular Formula:C₁₀H₁₀O₂
Molecular Weight:162.188
Hs Code.:
Mol file:41397-71-1.mol

Synonyms:(2Z)-3-(2-methylphenyl)propenoic acid

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Chemical Property of (2Z)-3-(2-methylphenyl)propenoic acid Edit

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Technology Process of (2Z)-3-(2-methylphenyl)propenoic acid

There total 45 articles about (2Z)-3-(2-methylphenyl)propenoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 615-37-2
ortho-methylphenyl iodide

: 79-10-7
acrylic acid

: 939-57-1,2373-76-4,41397-71-1
(E)-3-(2-methylphenyl)acrylic acid

Guidance literature:: With potassium hydroxide; PS-PEG-NH-C(O)C6H4PPh2-PdCl(η³-C3H5); at 50 ℃;
DOI:10.1055/s-2002-35605

Reference yield: 91.0%

: 201230-82-2
carbon monoxide

: 889869-30-1
trans-1-(2-bromovinyl)-2-methylbenzene

: 939-57-1,2373-76-4,41397-71-1
(E)-3-(2-methylphenyl)acrylic acid

Guidance literature:: With [bmim]PF₆; triethylamine; bis-triphenylphosphine-palladium(II) chloride; In water; at 100 ℃; for 20h; under 15001.2 Torr;
DOI:10.1021/jo052651p

Reference yield: 90.0%

: 64-18-6
formic acid

: C₉H₉I

: 939-57-1,2373-76-4,41397-71-1
(E)-3-(2-methylphenyl)acrylic acid

Guidance literature:: With palladium diacetate; triethylamine; dicyclohexyl-carbodiimide; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In N,N-dimethyl-formamide; at 100 ℃; for 20h; Inert atmosphere; Sealed tube;
DOI:10.1021/acs.joc.7b01808