Technology Process of (+)-(S)-2-sec-butylphenol
There total 9 articles about (+)-(S)-2-sec-butylphenol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydroxide;
In
ethanol; water;
for 3h;
Inert atmosphere;
Reflux;
DOI:10.1021/ja110052n
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: 2,2'-azobis(isobutyronitrile) / benzene / 0.5 h / Inert atmosphere
1.2: 3 h / 70 °C / Inert atmosphere
2.1: sodium hydroxide / ethanol; water / 3 h / Inert atmosphere; Reflux
With
2,2'-azobis(isobutyronitrile); sodium hydroxide;
In
ethanol; water; benzene;
DOI:10.1021/ja110052n
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid / dichloromethane / 14 h / 60 °C / Inert atmosphere
2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.75 h / 0 °C / Inert atmosphere
3.1: triethylamine / dichloromethane / 2 h / 20 °C / Inert atmosphere
4.1: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran; acetonitrile / 0.75 h / 20 °C / Inert atmosphere
5.1: 2,2'-azobis(isobutyronitrile) / benzene / 0.5 h / Inert atmosphere
5.2: 3 h / 70 °C / Inert atmosphere
6.1: sodium hydroxide / ethanol; water / 3 h / Inert atmosphere; Reflux
With
1H-imidazole; lithium aluminium tetrahydride; 2,2'-azobis(isobutyronitrile); iodine; triethylamine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; trifluoroacetic acid; sodium hydroxide;
In
tetrahydrofuran; ethanol; dichloromethane; water; acetonitrile; benzene;
DOI:10.1021/ja110052n