Technology Process of (S)-3-sec-butyl-2-hydroxy-5-iodobenzaldehyde
There total 10 articles about (S)-3-sec-butyl-2-hydroxy-5-iodobenzaldehyde which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
Iodine monochloride;
In
acetic acid;
for 4h;
Reflux;
Inert atmosphere;
DOI:10.1021/ja110052n
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium hydroxide / ethanol; water / 3 h / Inert atmosphere; Reflux
2: triethylamine; magnesium chloride / tetrahydrofuran / 2 h / Inert atmosphere; Reflux
3: Iodine monochloride / acetic acid / 4 h / Reflux; Inert atmosphere
With
Iodine monochloride; triethylamine; sodium hydroxide; magnesium chloride;
In
tetrahydrofuran; ethanol; water; acetic acid;
DOI:10.1021/ja110052n
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triethylamine; magnesium chloride / tetrahydrofuran / 2 h / Inert atmosphere; Reflux
2: Iodine monochloride / acetic acid / 4 h / Reflux; Inert atmosphere
With
Iodine monochloride; triethylamine; magnesium chloride;
In
tetrahydrofuran; acetic acid;
DOI:10.1021/ja110052n
