V₄O₂(O₂CC₂H₅)7(C₅H₄NCOO)2^(1-)*N(C₂H₅)4⁽¹⁺⁾=(N(C₂H₅)4)[V₄O₂(O₂CC₂H₅)7(C₅H₄NCOO)2]

Base Information

• Chemical Name: V₄O₂(O₂CC₂H₅)7(C₅H₄NCOO)2^(1-)*N(C₂H₅)4⁽¹⁺⁾=(N(C₂H₅)4)[V₄O₂(O₂CC₂H₅)7(C₅H₄NCOO)2]
• CAS No.: 202535-06-6
• Molecular Formula: C₈H₂₀N*C₃₃H₄₃N₂O₂₀V₄
• Molecular Weight: 1121.73
• Mol file: 202535-06-6.mol

Synonyms:V₄O₂(O₂CC₂H₅)7(C₅H₄NCOO)2^(1-)*N(C₂H₅)4⁽¹⁺⁾=(N(C₂H₅)4)[V₄O₂(O₂CC₂H₅)7(C₅H₄NCOO)2]

Chemical Property of V₄O₂(O₂CC₂H₅)7(C₅H₄NCOO)2^(1-)*N(C₂H₅)4⁽¹⁺⁾=(N(C₂H₅)4)[V₄O₂(O₂CC₂H₅)7(C₅H₄NCOO)2]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of V₄O₂(O₂CC₂H₅)7(C₅H₄NCOO)2^(1-)*N(C₂H₅)4⁽¹⁺⁾=(N(C₂H₅)4)[V₄O₂(O₂CC₂H₅)7(C₅H₄NCOO)2]

There total 1 articles about V₄O₂(O₂CC₂H₅)7(C₅H₄NCOO)2^(1-)*N(C₂H₅)4⁽¹⁺⁾=(N(C₂H₅)4)[V₄O₂(O₂CC₂H₅)7(C₅H₄NCOO)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

Vanadium (III) chloride-(tris-tetrahydrofuran) (131063-11-1,16997-51-6,19559-06-9) + tetraethylammonium chloride (56-34-8) + sodium proprionate (137-40-6) + sodium picolinate (57665-05-1) → V4O2(O2CC2H5)7(C5H4NCOO)2(1-)*N(C2H5)4(1+)=(N(C2H5)4)[V4O2(O2CC2H5)7(C5H4NCOO)2] (202535-06-6) + sodium chloride (7647-14-5)

Guidance literature:

In acetonitrile; inert atmosphere, Schlenk techniques; aq. Na(pic) soln. addn. to stirred mixt. of V-compd., NaO2CEt and MeCN, stirring overnight, NaCl ppt. filtration off, NEt4Cl addn. to filtrate, solvent removal (vac.), residue redissoln. (acetone), THF addn.; pptn. after a few on standing at room temp., ppt. filtration off, washing (THF), vac. drying; elem. anal.;

DOI:10.1021/ja9732439

upstream raw materials:

Vanadium (III) chloride-(tris-tetrahydrofuran)

tetraethylammonium chloride

sodium proprionate

sodium picolinate

Refernces