C₂₃H₃₆N₄O₁₂

Base Information

• Chemical Name: C₂₃H₃₆N₄O₁₂
• CAS No.: 1422541-00-1
• Molecular Formula: C₂₃H₃₆N₄O₁₂
• Molecular Weight: 560.558
• Mol file: 1422541-00-1.mol

Synonyms:C₂₃H₃₆N₄O₁₂

Chemical Property of C₂₃H₃₆N₄O₁₂

Chemical Property:

Purity/Quality:

>98.00% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₃H₃₆N₄O₁₂

There total 3 articles about C₂₃H₃₆N₄O₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

4-Nitrophenyl chloroformate (7693-46-1) + α-(2-azidoethyl)-ω-hydroxyhexa(oxyethylene) (352439-36-2) → C23H36N4O12 (1422541-00-1)

Guidance literature:

In acetonitrile; at 0 - 20 ℃;

DOI:10.1039/c2ob26968f

Reference yield:

octaethylene glycol (5117-19-1) → C23H36N4O12 (1422541-00-1)

Guidance literature:

Multi-step reaction with 3 steps

1: silver(l) oxide / dichloromethane / 24 h / 0 - 20 °C

2: sodium azide / N,N-dimethyl-formamide / 12 h / 65 °C

3: acetonitrile / 0 - 20 °C

With sodium azide; silver(l) oxide; In dichloromethane; N,N-dimethyl-formamide; acetonitrile;

DOI:10.1039/c2ob26968f

Reference yield:

23-hydroxy-3,6,9,12,15,18,21-heptaoxatricos-1-yl methanesulfonate (924895-57-8) → C23H36N4O12 (1422541-00-1)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium azide / N,N-dimethyl-formamide / 12 h / 65 °C

2: acetonitrile / 0 - 20 °C

With sodium azide; In N,N-dimethyl-formamide; acetonitrile;

DOI:10.1039/c2ob26968f

upstream raw materials:

4-Nitrophenyl chloroformate

α-(2-azidoethyl)-ω-hydroxyhexa(oxyethylene)

octaethylene glycol

23-hydroxy-3,6,9,12,15,18,21-heptaoxatricos-1-yl methanesulfonate

Refernces