Sodium 2-nitrophenoxide

Base Information

• Chemical Name: Sodium 2-nitrophenoxide
• CAS No.: 824-39-5
• Molecular Formula: C6H4NNaO3
• Molecular Weight: 161.092
• Hs Code.: 2908999090
• Mol file: 824-39-5.mol

Synonyms:Sodium o-nitrophenol;Sodium o-nitrophenolate;Sodiumo-nitrophenoxide;o-Nitrophenol sodium salt;Sodium ortho-nitrophenolate(98%TC);Phenol,2-nitro-, sodium salt (9CI);Phenol, o-nitro-, sodium deriv. (6CI);Phenol,o-nitro-, sodium salt (8CI);Sodium, (o-nitrophenoxy)- (7CI);(o-Nitrophenolato)sodium;2-Nitrophenol sodium salt;Sodium 2-nitrophenolate;

Chemical Property of Sodium 2-nitrophenoxide

Chemical Property:

• Appearance/Colour: dark red acicular crystals
• Vapor Pressure: 0.0987mmHg at 25°C
• Melting Point: 215-218°C
• Boiling Point: 215.8 °C at 760 mmHg
• Flash Point: 97.1 °C
• PSA: 68.88000
• Density: 1.301
• LogP: 2.26180
• Storage Temp.: Sealed in dry,Room Temperature
• Solubility.: DMSO (Slightly), Methanol (Slightly)

Purity/Quality:

99% ^*data from raw suppliers

Sodium2-Nitrophenolate ^*data from reagent suppliers

Safty Information:

• Pictogram(s): T,Xi
• Hazard Codes: T,Xi

MSDS Files:

Useful:

Technology Process of Sodium 2-nitrophenoxide

There total 9 articles about Sodium 2-nitrophenoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-Chloronitrobenzene (88-73-3) → sodium o-nitrophenate (824-39-5)

Guidance literature:

With sodium hydroxide; at 160 - 175 ℃; for 4.5h; under 51005.1 - 54005.4 Torr; Large scale;

Reference yield:

2-hydroxynitrobenzene (88-75-5,78813-12-4) → sodium o-nitrophenate (824-39-5)

Guidance literature:

With sodium hydroxide; In ethanol;

Reference yield:

1,2-Dinitrobenzene (528-29-0) → sodium o-nitrophenate (824-39-5)

Guidance literature:

With sodium hydroxide; dihydrogen peroxide; In 1,4-dioxane; water; at 30 ℃; for 2.5h; Rate constant; Mechanism; var. times; dependence on H₂O₂ concentration; intermediate;

upstream raw materials:

methyl-(2-nitro-phenyl)-sulfoxide

1-nitro-2-(phenylsulfinyl)benzene

1-(methylsulfonyl)-2-nitrobenzene

1-nitro-2-(phenylsulfonyl)benzene

Downstream raw materials:

1,6-bis(2-nitrophenyl)-1,6-dioxahexane

mononitrophenyl carbonate

5-nitro-2-(2-nitro-phenoxy)-pyridine

n-butyl o-nitrophenyl ether

Refernces

• 1、 Hanprasit, Sasikarn,Tungkijanansin, Nuttanee,Prompawilai, Arisa,Eangpayung, Supattra,Ervithayasuporn, Vuthichai. "Synthesis and isolation of non-chromophore cage-rearranged silsesquioxanes from base-catalyzed reactions". supporting information. p. 16117 - 16120. Retrieved 2016/10/31.
• 2、 Heilporn, S.,Broeders, F.,Daloze, D.,Braekman, J. C.,Boeynaems, J. M.. "SYNTHESIS OF BAPTA-AM ANALOGUES CAPABLE OF ENHANCING THE VASCULAR PRODUCTION OF PROSTACYCLIN". . p. 309 - 320. Retrieved 2007/10/02.