TRIALLYLSILANE

Base Information

• Chemical Name: TRIALLYLSILANE
• CAS No.: 1116-62-7
• Molecular Formula: C9H16Si
• Molecular Weight: 152.31
• Hs Code.: 2931900090
• Mol file: 1116-62-7.mol

Synonyms:Silane,tri-2-propenyl- (9CI);Silane, triallyl- (6CI,7CI,8CI);Triallylsilane;

Chemical Property of TRIALLYLSILANE

Chemical Property:

• Appearance/Colour: clear colorless liquid
• Vapor Pressure: 2.34mmHg at 25°C
• Refractive Index: 1.471-1.474
• Boiling Point: 166.5 °C at 760 mmHg
• Flash Point: 49.7 °C
• PSA: 0.00000
• LogP: 2.77150

Purity/Quality:

98%,99%, ^*data from raw suppliers

TRIALLYLSILANE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38-10
• Safety Statements: 37/39-26-16

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of TRIALLYLSILANE

There total 5 articles about TRIALLYLSILANE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.3%

allylmagnesium bromide (2622-05-1) → Triallylsilane (1116-62-7)

Guidance literature:

With trichlorosilane; 3-chloroprop-1-ene; In diethyl ether; for 3h; Heating;

Reference yield: 27.5%

allylmagnesium bromide (2622-05-1) + chloromethylmethyldichlorosilane (1558-33-4) → Triallylsilane (1116-62-7) + Diallyl-but-3-enyl-methyl-silane

Guidance literature:

With 3-chloroprop-1-ene; In tetrahydrofuran; for 3h; Heating;

Reference yield:

allylmagnesium bromide (1730-25-2) → Triallylsilane (1116-62-7)

Guidance literature:

With diethyl ether; trichlorosilane;

DOI:10.1021/jo01164a013

upstream raw materials:

allylmagnesium bromide

allylmagnesium bromide

chloromethylmethyldichlorosilane

trichlorosilane

Downstream raw materials:

4-(tert-Butyldimethylsiloxy)triallylsilylbenzene

4-(Triallylsiloxy)bromobenzene

4-(Triallylsilyl)phenol

Refernces

• 1、 Zhun', V.I.,Tsvetkov, A. L.,Sheludyakov, V. D.,Lavygin, I. A.,Leitan, O. V.,et al.. "SYNTHESIS, MASS SPECTRA, AND PHYSICAL PROPERTIES OF ALLYLSILANES". . p. 1425 - 1431. Retrieved 2007/10/02.