C₁₇H₁₄F₃NO₃

Base Information Edit

Chemical Name:C₁₇H₁₄F₃NO₃
CAS No.:1380243-46-8
Molecular Formula:C₁₇H₁₄F₃NO₃
Molecular Weight:337.298
Hs Code.:
Mol file:1380243-46-8.mol

C<sub>17</sub>H<sub>14</sub>F<sub>3</sub>NO<sub>3</sub>

Synonyms:C₁₇H₁₄F₃NO₃

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Chemical Property of C₁₇H₁₄F₃NO₃ Edit

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Technology Process of C₁₇H₁₄F₃NO₃

There total 7 articles about C₁₇H₁₄F₃NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1380243-43-5
C₁₇H₁₆F₃NO₂

: 1380243-46-8
C₁₇H₁₄F₃NO₃

Guidance literature:: With sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; sodium bromide; In dichloromethane; at 0 ℃; for 2h;

Reference yield:

: 98-88-4
benzoyl chloride

: 1380243-46-8
C₁₇H₁₄F₃NO₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: triethylamine / dichloromethane / 12 h / 0 - 20 °C

2.1: sodium tetrahydroborate; iodine; methanol / tetrahydrofuran / 2 h / 0 - 5 °C / Reflux

3.1: triethylamine / dichloromethane / 4 h / 0 - 20 °C

4.1: sodium hydride / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere

5.1: isopropylmagnesium bromide / tetrahydrofuran / -20 °C / Inert atmosphere

5.2: 0.25 h / -5 °C / Inert atmosphere

5.3: 0.08 h

6.1: methyl iodide / water; methanol / 0.5 h / 20 °C / Cooling with ice

6.2: pH 3 - Ca_. 7 / Reflux

7.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hypochlorite; sodium bromide; sodium hydrogencarbonate / dichloromethane / 2 h / 0 °C

7.2: pH 2 - 3

With methanol; sodium hypochlorite; sodium tetrahydroborate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; iodine; isopropylmagnesium bromide; sodium hydride; sodium hydrogencarbonate; triethylamine; sodium bromide; methyl iodide; In tetrahydrofuran; methanol; dichloromethane; water;

Reference yield:

: 10290-61-6
(S)-N-benzoylmethionine

: 1380243-46-8
C₁₇H₁₄F₃NO₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium tetrahydroborate; iodine; methanol / tetrahydrofuran / 2 h / 0 - 5 °C / Reflux

2.1: triethylamine / dichloromethane / 4 h / 0 - 20 °C

3.1: sodium hydride / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere

4.1: isopropylmagnesium bromide / tetrahydrofuran / -20 °C / Inert atmosphere

4.2: 0.25 h / -5 °C / Inert atmosphere

4.3: 0.08 h

5.1: methyl iodide / water; methanol / 0.5 h / 20 °C / Cooling with ice

5.2: pH 3 - Ca_. 7 / Reflux

6.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hypochlorite; sodium bromide; sodium hydrogencarbonate / dichloromethane / 2 h / 0 °C

6.2: pH 2 - 3

With methanol; sodium hypochlorite; sodium tetrahydroborate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; iodine; isopropylmagnesium bromide; sodium hydride; sodium hydrogencarbonate; triethylamine; sodium bromide; methyl iodide; In tetrahydrofuran; methanol; dichloromethane; water;