DICYCLOHEXYLPHOSPHINYL CHLORIDE

Base Information

• Chemical Name: DICYCLOHEXYLPHOSPHINYL CHLORIDE
• CAS No.: 15873-72-0
• Molecular Formula: C12H22 Cl O P
• Molecular Weight: 248.733
• Hs Code.: 2903890090
• Mol file: 15873-72-0.mol

Synonyms:Phosphinicchloride, dicyclohexyl- (8CI,9CI); Chlorobis(cyclohexyl)phosphine oxide

Chemical Property of DICYCLOHEXYLPHOSPHINYL CHLORIDE

Chemical Property:

• Melting Point: 109 °C
• Boiling Point: 395oC at 760 mmHg
• Flash Point: 192.7oC
• PSA: 26.88000
• Density: 1.09g/cm3
• LogP: 5.16870
• Storage Temp.: Refrigerator

Purity/Quality:

98%,99%, ^*data from raw suppliers

Dicyclohexylphosphinyl Chloride >98.0%(GC)(T) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of DICYCLOHEXYLPHOSPHINYL CHLORIDE

There total 5 articles about DICYCLOHEXYLPHOSPHINYL CHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dicyclohexylphosphinic acid (832-39-3) → dicyclohexylphosphinoyl chloride (15873-72-0)

Guidance literature:

With thionyl chloride;

DOI:10.1002/zaac.19542770505

Reference yield:

dicyclohexylphosphine oxide (14717-29-4) → dicyclohexylphosphinoyl chloride (15873-72-0)

Guidance literature:

With chlorine; In cyclohexane; Irradiation;

Reference yield:

cyclohexylmagnesiumchloride (931-51-1) → dicyclohexylphosphinoyl chloride (15873-72-0)

Guidance literature:

Multi-step reaction with 2 steps

1: POCl₃

2: SOCl₂

With thionyl chloride; trichlorophosphate;

DOI:10.1002/zaac.19542770505

upstream raw materials:

dicyclohexylphosphinic acid

dicyclohexylphosphine oxide

cyclohexane

cyclohexylphosphonic dichloride

Downstream raw materials:

p-fluoroaniline hydrochloride

m-toluidine hydrochloride

3-chloroaniline hydrochloride

aniline hydrochloride

Refernces

• 1、 -. "Preparation of 3-substituted cephalosporins". . . Retrieved 2008/06/13.