Technology Process of 2-(4-methoxyphenyl)-3-methyl-3H-imidazo[4,5-b]pyridine
There total 3 articles about 2-(4-methoxyphenyl)-3-methyl-3H-imidazo[4,5-b]pyridine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper(l) iodide; palladium diacetate; caesium carbonate;
In
N,N-dimethyl-formamide;
at 200 ℃;
for 0.5h;
Temperature;
Time;
regioselective reaction;
Inert atmosphere;
Microwave irradiation;
DOI:10.1039/c3ob27477b
- Guidance literature:
-
Multi-step reaction with 2 steps
1: acetic acid / dichloromethane / 0.5 h / 150 °C / Microwave irradiation
2: palladium diacetate; copper(l) iodide; caesium carbonate / N,N-dimethyl-formamide / 0.5 h / 200 °C / Inert atmosphere; Microwave irradiation
With
copper(l) iodide; palladium diacetate; caesium carbonate; acetic acid;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c3ob27477b
- Guidance literature:
-
Multi-step reaction with 3 steps
1: palladium 10% on activated carbon; hydrazine hydrate / 1,2-dimethoxyethane / 1.5 h / 40 °C / Inert atmosphere; Reflux
2: acetic acid / dichloromethane / 0.5 h / 150 °C / Microwave irradiation
3: palladium diacetate; copper(l) iodide; caesium carbonate / N,N-dimethyl-formamide / 0.5 h / 200 °C / Inert atmosphere; Microwave irradiation
With
copper(l) iodide; palladium 10% on activated carbon; palladium diacetate; caesium carbonate; hydrazine hydrate; acetic acid;
In
1,2-dimethoxyethane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c3ob27477b