O-(2,4-dinitrophenyl)-N,N-diethylhydroxylamine

Base Information

• Chemical Name: O-(2,4-dinitrophenyl)-N,N-diethylhydroxylamine
• CAS No.: 29746-98-3
• Molecular Formula: C₁₀H₁₃N₃O₅
• Molecular Weight: 255.23
• Mol file: 29746-98-3.mol

Synonyms:O-(2,4-dinitrophenyl)-N,N-diethylhydroxylamine

Chemical Property of O-(2,4-dinitrophenyl)-N,N-diethylhydroxylamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of O-(2,4-dinitrophenyl)-N,N-diethylhydroxylamine

There total 2 articles about O-(2,4-dinitrophenyl)-N,N-diethylhydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

N-ethyl-N-hydroxy-ethanamine (3710-84-7) + 2,4-Dinitrofluorobenzene (70-34-8,65727-75-5) → O-(2,4-dinitrophenyl)-N,N-diethylhydroxylamine (29746-98-3)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃;

DOI:10.1002/anie.201708693

Reference yield:

→ O-(2,4-dinitrophenyl)-N,N-diethylhydroxylamine (29746-98-3)

Guidance literature:

Natrium-2,4-dinitrophenolat, N-Chlordiethylamin, 5 Std. bei 35-45grad;

Reference yield: 91.0%

naphthalene (91-20-3,71998-51-1,72931-45-4) + O-(2,4-dinitrophenyl)-N,N-diethylhydroxylamine (29746-98-3) → N,N-diethyl-1-naphthylamine (84-95-7)

Guidance literature:

With perchloric acid; tris(2,2'-bipyridyl)ruthenium dichloride; In water; acetonitrile; at 20 ℃; Sealed tube; Inert atmosphere; Irradiation;

DOI:10.1002/anie.201708693

upstream raw materials:

N-ethyl-N-hydroxy-ethanamine

2,4-Dinitrofluorobenzene

Downstream raw materials:

N,N-diethyl-1-naphthylamine

N,N-diethylaniline

Refernces