Technology Process of 3-(3-Butenyl)anisic Acid
There total 3 articles about 3-(3-Butenyl)anisic Acid which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium tert-butylate / tert-butyl alcohol / 24 h / 90 °C
2: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / 1) in dry ether at reflux for 1h 2) CO2 as a continous stream for 1h
With
n-butyllithium; N,N,N,N,-tetramethylethylenediamine; potassium tert-butylate;
In
tert-butyl alcohol;
DOI:10.1021/jo00317a027
- Guidance literature:
-
Multi-step reaction with 3 steps
1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / 1) in dry ether at reflux for 1h 2) -22 deg C overnight
2: potassium tert-butylate / tert-butyl alcohol / 24 h / 90 °C
3: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / 1) in dry ether at reflux for 1h 2) CO2 as a continous stream for 1h
With
n-butyllithium; N,N,N,N,-tetramethylethylenediamine; potassium tert-butylate;
In
tert-butyl alcohol;
DOI:10.1021/jo00317a027
- Guidance literature:
-
With
n-butyllithium; N,N,N,N,-tetramethylethylenediamine;
Yield given. Multistep reaction;
1) in dry ether at reflux for 1h 2) CO2 as a continous stream for 1h;
DOI:10.1021/jo00317a027
