sodium perfluoroheptanoate

Base Information

• Chemical Name: sodium perfluoroheptanoate
• CAS No.: 20109-59-5
• Molecular Formula: C7H F13 O2 . Na
• Molecular Weight: 386.045
• Hs Code.: 2915900090
• Mol file: 20109-59-5.mol

Synonyms:Heptanoicacid, tridecafluoro-, sodium salt (8CI,9CI); Sodium perfluoroenanthate; Sodiumperfluoroheptanoate; Sodium tridecafluoroheptanoate

Chemical Property of sodium perfluoroheptanoate

Chemical Property:

• Vapor Pressure: 0.539mmHg at 25°C
• Boiling Point: 175.8°Cat760mmHg
• Flash Point: 51.3°C
• PSA: 40.13000
• Density: 1.735g/cm³
• LogP: 2.47510

Purity/Quality:

98%Min ^*data from raw suppliers

Sodium perfluoroheptanoate 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of sodium perfluoroheptanoate

There total 4 articles about sodium perfluoroheptanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

perfluoroheptyl iodide (335-58-0) → perfluoro-1H-heptane (375-83-7) + perfluoroheptanoic acid sodium salt (20109-59-5)

Guidance literature:

With rongalite; sodium hydrogencarbonate; In water; N,N-dimethyl-formamide; at 90 ℃; for 18h;

DOI:10.1016/S0022-1139(00)82053-9

Reference yield: 78.0%

1-bromopentadecafluoroheptane (375-88-2) → perfluoro-1H-heptane (375-83-7) + perfluoroheptanoic acid sodium salt (20109-59-5)

Guidance literature:

With rongalite; In water; dimethyl sulfoxide; at 80 - 85 ℃; for 25h;

DOI:10.1016/S0022-1139(00)82053-9

Reference yield: 50.0%

methyl perfluoroheptanoate (14312-89-1) + Sodium salt of Benzamidoxime (65809-34-9) → perfluoroheptanoic acid sodium salt (20109-59-5) + N-hydroxybenzenecarboximidamide (613-92-3) + 5-perfluorohexyl-3-phenyl-1,2,4-oxadiazole

Guidance literature:

In toluene; at 80 - 90 ℃; for 10h;

DOI:10.1007/BF00698437

upstream raw materials:

1-bromopentadecafluoroheptane

perfluoroheptyl iodide

methyl perfluoroheptanoate

Sodium salt of Benzamidoxime

Downstream raw materials:

perfluoroheptanoyl chloride

perfluoroheptanoic acid

dodecafluoro-hex-2-ene

perfluoro-1-hexene

Refernces

• 1、 Il'in, V. V.,Kabakchi, E. V.,Ignatenko, A. V.. "Reactions of benzamidoxime and its sodium salt with methyl esters of fluorinated acids". . p. 485 - 487. Retrieved 1993.