Technology Process of benzyl 7-chlorocarbonyl-2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptanoate
There total 3 articles about benzyl 7-chlorocarbonyl-2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptanoate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
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1967-93-7
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioyl dichloride
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1355356-58-9
benzyl 7-chlorocarbonyl-2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptanoate
- Guidance literature:
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at 100 ℃;
for 2h;
Inert atmosphere;
Cooling with ice;
DOI:10.1016/j.bmc.2011.11.041
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678-45-5
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioic acid
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1355356-58-9
benzyl 7-chlorocarbonyl-2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptanoate
- Guidance literature:
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Multi-step reaction with 2 steps
1: thionyl chloride; N,N-dimethyl-formamide / 4 h / Inert atmosphere; Reflux
2: 2 h / 100 °C / Inert atmosphere; Cooling with ice
With
thionyl chloride; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2011.11.041
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678-45-5
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioic acid
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-
1355356-58-9
benzyl 7-chlorocarbonyl-2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptanoate
- Guidance literature:
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2,2,3,3,4,4,5,5,6,6,7,7-dodecafluorooctanedioic acid;
With
thionyl chloride;
In
N,N-dimethyl-formamide;
benzyl alcohol;
DOI:10.1016/j.bmcl.2017.02.050