N-pentylpyrrolidine

Base Information

• Chemical Name: N-pentylpyrrolidine
• CAS No.: 35152-38-6
• Molecular Formula: C₉H₁₉N
• Molecular Weight: 141.257
• Mol file: 35152-38-6.mol

Synonyms:N-pentylpyrrolidine

Chemical Property of N-pentylpyrrolidine

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of N-pentylpyrrolidine

There total 4 articles about N-pentylpyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,4-dioxane (123-91-1,28347-88-8,28347-91-3,39449-24-6,54841-74-6) + N,N'-dipentyl-L-tartaramide (7770-68-5) → N-pentylpyrrolidine (35152-38-6) + n-Pentylamine (110-58-7) + Di-n-amylamine (2050-92-2)

Guidance literature:

at 250 - 260 ℃; bei der Druckhydrierung_.Hydrogenation;

DOI:10.1021/ja01876a012

Reference yield:

5-hydroxy-1-(pyrrolidin-1-yl)pentan-1-one (73200-35-8) → N-pentylpyrrolidine (35152-38-6) + 1-(pyrrolidin-1-yl)pentan-1-one (4419-57-2)

Guidance literature:

With hydrogen; In 1,2-dimethoxyethane; at 160 ℃; for 20h; under 22502.3 Torr; Inert atmosphere; Autoclave; Molecular sieve;

DOI:10.1002/anie.201207803

Reference yield:

1-(pyrrolidin-1-yl)pent-4-yn-1-one (13991-18-9) → N-pentylpyrrolidine (35152-38-6) + 1-(pyrrolidin-1-yl)pentan-1-one (4419-57-2)

Guidance literature:

With hydrogen; In 1,2-dimethoxyethane; at 160 ℃; for 20h; under 22502.3 Torr; Inert atmosphere; Autoclave; Molecular sieve;

DOI:10.1002/anie.201207803

upstream raw materials:

1,4-dioxane

N,N'-dipentyl-malamide

N,N'-dipentyl-L-tartaramide

5-hydroxy-1-(pyrrolidin-1-yl)pentan-1-one

Downstream raw materials:

1-pentyl-1-(4-phenylazo-benzyl)-pyrrolidinium; bromide

1-pentyl-1H-pyrrole

diquat dibromide

N-butylpentylamine

Refernces