1,3-Diazidopropane

Base Information

• Chemical Name: 1,3-Diazidopropane
• CAS No.: 100910-72-3
• Molecular Formula: C3H6N6
• Molecular Weight: 126.121
• DSSTox Substance ID: DTXSID40591467
• Nikkaji Number: J1.495.290J
• Wikidata: Q82485240
• Mol file: 100910-72-3.mol

Synonyms:1,3-diazidopropane;100910-72-3;SCHEMBL15338512;DTXSID40591467

Chemical Property of 1,3-Diazidopropane

Chemical Property:

• XLogP3: 2.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 4
• Exact Mass: 126.06539422
• Heavy Atom Count: 9
• Complexity: 132

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C(CN=[N+]=[N-])CN=[N+]=[N-]

Technology Process of 1,3-Diazidopropane

There total 1 articles about 1,3-Diazidopropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S)-Glycidyl tosylate (70987-78-9,6746-81-2) → 1,3-diazido-propane (100910-72-3) + (R)-2-(azidomethyl)oxirane (681225-56-9,80044-10-6)

Guidance literature:

With sodium azide; In N,N-dimethyl-formamide; at 60 ℃; for 1h;

Reference yield: 96.0%

1,3-diazido-propane (100910-72-3) + 1-phenoxy-2-propyne (13610-02-1) → 1,3-bis[4-(phenoxymethyl)-1H-1,2,3-triazol-1-yl]propane (1356336-82-7)

Guidance literature:

With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In tetrahydrofuran; water; at 20 ℃; for 16h; Inert atmosphere;

DOI:10.1055/s-0031-1289573

Reference yield: 94.0%

1,3-diazido-propane (100910-72-3) + phenylacetylene (536-74-3) → 1,3-bis(4-phenyl-1H-1,2,3-triazol-1-yl)propane

Guidance literature:

With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In water; tert-butyl alcohol; at 40 ℃; Inert atmosphere;

DOI:10.2174/1573406414666181024111522

upstream raw materials:

(S)-Glycidyl tosylate

Downstream raw materials:

N,N'-(diphenyl)-1,3-diaminopropane dihydrochloride

3-azidopropylamine

N,N'-diphenylpropane-1,3-diamine

C₃₁H₃₄N₆

Refernces