Technology Process of t-butyl <4-(2-oxopropyl)-2-oxoazetidin-1-yl>triphenylphosphoranylideneacetate
There total 7 articles about t-butyl <4-(2-oxopropyl)-2-oxoazetidin-1-yl>triphenylphosphoranylideneacetate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) mercury(II) acetate, 2.) copper(II) chloride dihydrate, palladium(II) chloride / 1) methanol, 2 h, room temperature; 2) methanol, 1 h, 60 deg C
2: benzene / 4 h / Heating
3: 1.) 2,6-lutidine, 2.) thionyl chloride / 1) THF, -20 deg C; 2) 20 min
4: 0.255 g / 2,6-lutidine / dioxane / 16 h / Ambient temperature
With
2,6-dimethylpyridine; thionyl chloride; mercury(II) diacetate; copper dichloride; palladium dichloride;
In
1,4-dioxane; benzene;
DOI:10.1039/P19810003242
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 16.05 g / 72 h / Ambient temperature
2: 1.) mercury(II) acetate, 2.) copper(II) chloride dihydrate, palladium(II) chloride / 1) methanol, 2 h, room temperature; 2) methanol, 1 h, 60 deg C
3: benzene / 4 h / Heating
4: 1.) 2,6-lutidine, 2.) thionyl chloride / 1) THF, -20 deg C; 2) 20 min
5: 0.255 g / 2,6-lutidine / dioxane / 16 h / Ambient temperature
With
2,6-dimethylpyridine; thionyl chloride; mercury(II) diacetate; copper dichloride; palladium dichloride;
In
1,4-dioxane; benzene;
DOI:10.1039/P19810003242
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1.) 2,6-lutidine, 2.) thionyl chloride / 1) THF, -20 deg C; 2) 20 min
2: 0.255 g / 2,6-lutidine / dioxane / 16 h / Ambient temperature
With
2,6-dimethylpyridine; thionyl chloride;
In
1,4-dioxane;
DOI:10.1039/P19810003242
