Diphenyl-(4-methoxy-phenyl)-<2,7-dibrom-fluorenyliden-(9)>-phosphoran

Base Information

• Chemical Name: Diphenyl-(4-methoxy-phenyl)-<2,7-dibrom-fluorenyliden-(9)>-phosphoran
• CAS No.: 24764-33-8
• Molecular Formula: C₃₂H₂₃Br₂OP
• Molecular Weight: 614.316
• Mol file: 24764-33-8.mol

Synonyms:

Chemical Property of Diphenyl-(4-methoxy-phenyl)-<2,7-dibrom-fluorenyliden-(9)>-phosphoran

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Diphenyl-(4-methoxy-phenyl)-<2,7-dibrom-fluorenyliden-(9)>-phosphoran

There total 2 articles about Diphenyl-(4-methoxy-phenyl)-<2,7-dibrom-fluorenyliden-(9)>-phosphoran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,7-dibromo-9H-fluorene (16433-88-8) → Diphenyl-(4-methoxy-phenyl)-<2,7-dibrom-fluorenyliden-(9)>-phosphoran (24764-33-8)

Guidance literature:

Multi-step reaction with 2 steps

1: Br₂ / CCl₄

2: (i) benzene, (ii) aq. NaOH, CHCl₃

With bromine; In tetrachloromethane;

Reference yield:

2,7,9-tribromofluorene (26279-24-3) + (4-methoxyphenyl)diphenylphosphane (896-89-9) → Diphenyl-(4-methoxy-phenyl)-<2,7-dibrom-fluorenyliden-(9)>-phosphoran (24764-33-8)

Guidance literature:

Multistep reaction; (i) benzene, (ii) aq. NaOH, CHCl₃;

upstream raw materials:

2,7,9-tribromofluorene

(4-methoxyphenyl)diphenylphosphane

2,7-dibromo-9H-fluorene