C₃₈H₄₀N₆O₆

Base Information

• Chemical Name: C₃₈H₄₀N₆O₆
• CAS No.: 120075-74-3
• Molecular Formula: C₃₈H₄₀N₆O₆
• Molecular Weight: 676.772
• Mol file: 120075-74-3.mol

Synonyms:

Chemical Property of C₃₈H₄₀N₆O₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₈H₄₀N₆O₆

There total 5 articles about C₃₈H₄₀N₆O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

3,6-dioxa-1,8-diaminooctane (929-59-9,892154-56-2) + 5-(benzyloxy)-4-chloro-6-methoxyquinazoline (120075-53-8) → C38H40N6O6 (120075-74-3)

Guidance literature:

With triethylamine; In ethanol; for 24h; Ambient temperature;

DOI:10.1248/cpb.36.3933

Reference yield:

2-(benzyloxy)-3-methoxy-6-nitrobenzaldehyde (2426-61-1) → C38H40N6O6 (120075-74-3)

Guidance literature:

Multi-step reaction with 5 steps

1: 71 percent / 10percent aq. potassium permanganate / acetone / 7 h / 40 °C

2: 79 percent / FeSO₄*7H₂O, 8M NH₄OH / H₂O / 0.5 h / Heating

3: 80 percent / piperidine / ethanol / 30 h / Heating

4: 80 percent / phosphoryl chloride, triethylamine / benzene / 3 h / 80 °C

5: 60 percent / triethylamine / ethanol / 24 h / Ambient temperature

With piperidine; ammonium hydroxide; potassium permanganate; iron(II) sulfate; triethylamine; trichlorophosphate; In ethanol; water; acetone; benzene;

DOI:10.1248/cpb.36.3933

Reference yield:

6-amino-2-benzyloxy-3-methoxybenzoic acid (120075-49-2) → C38H40N6O6 (120075-74-3)

Guidance literature:

Multi-step reaction with 3 steps

1: 80 percent / piperidine / ethanol / 30 h / Heating

2: 80 percent / phosphoryl chloride, triethylamine / benzene / 3 h / 80 °C

3: 60 percent / triethylamine / ethanol / 24 h / Ambient temperature

With piperidine; triethylamine; trichlorophosphate; In ethanol; benzene;

DOI:10.1248/cpb.36.3933

upstream raw materials:

3,6-dioxa-1,8-diaminooctane

5-(benzyloxy)-4-chloro-6-methoxyquinazoline

2-(benzyloxy)-3-methoxy-6-nitrobenzaldehyde

6-amino-2-benzyloxy-3-methoxybenzoic acid

Refernces