trans-bis(acetone methylphenylhydrazone)dichloropalladium(II)

Base Information

• Chemical Name: trans-bis(acetone methylphenylhydrazone)dichloropalladium(II)
• CAS No.: 52941-98-7
• Molecular Formula: C₂₀H₂₈Cl₂N₄Pd
• Molecular Weight: 501.795
• Mol file: 52941-98-7.mol

Synonyms:

Chemical Property of trans-bis(acetone methylphenylhydrazone)dichloropalladium(II)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of trans-bis(acetone methylphenylhydrazone)dichloropalladium(II)

There total 2 articles about trans-bis(acetone methylphenylhydrazone)dichloropalladium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

bis(benzonitrile)palladium(II) dichloride (15617-18-2,39958-10-6,14220-64-5) + acetone methylphenylhydrazone (3741-86-4) → trans-bis(acetone methylphenylhydrazone)dichloropalladium(II) (52941-98-7,55156-22-4)

Guidance literature:

In benzene;

DOI:10.1016/S0020-1693(00)81925-8

Reference yield:

bis(benzonitrile)palladium(II) chloride (14220-64-5,39958-10-6,15617-18-2) + Acetone dimethylhydrazone (13483-31-3) + acetone methylphenylhydrazone (3741-86-4) → trans-[PdCl2(Me2C=NNMe2)2] (63056-77-9) + trans-[PdCl2(Me2C=NNMePh)(Me2C=NNMe2)] (69419-34-7) + trans-bis(acetone methylphenylhydrazone)dichloropalladium(II) (52941-98-7,55156-22-4)

Guidance literature:

In dichloromethane; equimolar amts., room temp., 1 d; evapn., stirring with pentane (several h), high pressure chromy. (LiChrorosorb DIOL, hexane/CH2Cl2 85:15 v/v); elem. anal.;

DOI:10.1039/DT9790001262

upstream raw materials:

bis(benzonitrile)palladium(II) chloride

Acetone dimethylhydrazone

acetone methylphenylhydrazone

bis(benzonitrile)palladium(II) dichloride