Technology Process of tris(2,4-pentanedionato)ruthenium(III)
There total 45 articles about tris(2,4-pentanedionato)ruthenium(III) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium hydrogencarbonate;
In
water;
heating mixt. of aq. soln. of Ru complex and acetylacetone on water bath for 10 min, addn. of KHCO3, further heating on water bath for 2 h, cooling to room temp.; centrifugation, washing with water (crop I), concn. of mother liquor, sepn. as above (crop II), recrystn. from CH2Cl2/hexane;
- Guidance literature:
-
rhodium(III) chloride hydrate; acetylacetone;
In
water;
at 100 ℃;
for 0.25h;
Microwave irradiation;
With
sodium hydroxide;
In
water;
for 0.166667h;
pH=6 - 7;
Time;
Concentration;
DOI:10.1007/s11172-012-0318-9
- Guidance literature:
-
With
potassium hydroxide;
In
water;
heating mixt. of aq. soln. of Ru complex and acetylacetone on water bath for 10 min, addn. of KOH, further heating on water bath for 2 h, cooling to room temp.; centrifugation, washing with water (crop I), concn. of mother liquor, sepn. as above (crop II), recrystn. from CH2Cl2/hexane;
