2,3-DICHLORO-5,6-DIMETHOXYPHENYLAMINE

Base Information

• Chemical Name: 2,3-DICHLORO-5,6-DIMETHOXYPHENYLAMINE
• CAS No.: 101252-15-7
• Molecular Formula: C₈H₉Cl₂NO₂
• Molecular Weight: 222.071
• Mol file: 101252-15-7.mol

Synonyms:

Chemical Property of 2,3-DICHLORO-5,6-DIMETHOXYPHENYLAMINE

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,3-DICHLORO-5,6-DIMETHOXYPHENYLAMINE

There total 2 articles about 2,3-DICHLORO-5,6-DIMETHOXYPHENYLAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,2-dichloro-4,5-dimethoxy-3-nitro-benzene (117882-84-5) → 2,3-dichloro-5,6-dimethoxy-aniline (101252-15-7)

Guidance literature:

With hydrogenchloride; tin; acetic acid;

DOI:10.1039/jr9560003820

Reference yield:

4,5-Dichlor-brenzcatechindimethylether (2772-46-5) → 2,3-dichloro-5,6-dimethoxy-aniline (101252-15-7)

Guidance literature:

Multi-step reaction with 2 steps

1: acetic acid anhydride; aqueous HNO₃

2: tin; aqueous HCl; acetic acid

With hydrogenchloride; tin; nitric acid; acetic anhydride; acetic acid;

DOI:10.1039/jr9560003820

Reference yield:

2,3-dichloro-5,6-dimethoxy-aniline (101252-15-7) → 2,3-dimethoxyaniline (6299-67-8)

Guidance literature:

With potassium hydroxide; hydrogen; nickel; In methanol;

upstream raw materials:

1,2-dichloro-4,5-dimethoxy-3-nitro-benzene

4,5-Dichlor-brenzcatechindimethylether

Downstream raw materials:

2,3-dimethoxyaniline

2,3,2',3'-Tetrahydroxy-biphenyl

1-iodo-2,3-dimethoxybenzene