C₁₉H₂₀N₂O₈

Base Information

• Chemical Name: C₁₉H₂₀N₂O₈
• CAS No.: 1257321-39-3
• Molecular Formula: C₁₉H₂₀N₂O₈
• Molecular Weight: 404.376
• Mol file: 1257321-39-3.mol

Synonyms:

Chemical Property of C₁₉H₂₀N₂O₈

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₉H₂₀N₂O₈

There total 6 articles about C₁₉H₂₀N₂O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

isomyristicin (487-62-7) → C19H20N2O8 (1257321-39-3)

Guidance literature:

Multi-step reaction with 5 steps

1.1: pyridine; ozone / methanol; chloroform / -15 - 0 °C

2.1: ammonium hydroxide; iodine / tetrahydrofuran; water / 16 h / 20 °C

2.2: 4 h / Reflux

3.1: thionyl chloride / 3 h / Reflux

4.1: hydrazine hydrate / methanol / 6 h / Reflux

5.1: pyridine / dichloromethane / -20 - 20 °C

With pyridine; ammonium hydroxide; thionyl chloride; iodine; ozone; hydrazine hydrate; In tetrahydrofuran; methanol; dichloromethane; chloroform; water;

DOI:10.1021/np1004278

Reference yield:

myristicin (607-91-0) → C19H20N2O8 (1257321-39-3)

Guidance literature:

Multi-step reaction with 6 steps

1.1: tetrabutylammomium bromide; potassium hydroxide / 0.67 h / 100 °C

2.1: pyridine; ozone / methanol; chloroform / -15 - 0 °C

3.1: ammonium hydroxide; iodine / tetrahydrofuran; water / 16 h / 20 °C

3.2: 4 h / Reflux

4.1: thionyl chloride / 3 h / Reflux

5.1: hydrazine hydrate / methanol / 6 h / Reflux

6.1: pyridine / dichloromethane / -20 - 20 °C

With pyridine; ammonium hydroxide; thionyl chloride; tetrabutylammomium bromide; iodine; ozone; hydrazine hydrate; potassium hydroxide; In tetrahydrofuran; methanol; dichloromethane; chloroform; water;

DOI:10.1021/np1004278

Reference yield:

3-methoxy-4,5-methylenedioxybenzaldehyde (5780-07-4) → C19H20N2O8 (1257321-39-3)

Guidance literature:

Multi-step reaction with 4 steps

1.1: ammonium hydroxide; iodine / tetrahydrofuran; water / 16 h / 20 °C

1.2: 4 h / Reflux

2.1: thionyl chloride / 3 h / Reflux

3.1: hydrazine hydrate / methanol / 6 h / Reflux

4.1: pyridine / dichloromethane / -20 - 20 °C

With pyridine; ammonium hydroxide; thionyl chloride; iodine; hydrazine hydrate; In tetrahydrofuran; methanol; dichloromethane; water;

DOI:10.1021/np1004278

upstream raw materials:

isomyristicin

myristicin

5-methoxy-3,4-methylenedioxybenzoic acid

methyl 7-methoxybenzo[d][1,3]dioxole-5-carboxylate

Downstream raw materials:

2-(3,4,5-trimethoxyphenyl)-5-(3-methoxy-4,5-methylenedioxyphenyl)-1,3,4-oxadiazole

Refernces