Technology Process of 2-ethenyl-4,5-dimethoxybenzaldoxime O-methyl ether
There total 4 articles about 2-ethenyl-4,5-dimethoxybenzaldoxime O-methyl ether which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium hydride;
In
N,N-dimethyl-formamide;
1.) ice cooling, 30 min, 2.) room temperature, 1 h;
DOI:10.3987/COM-88-S12
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 85 percent / NH2OH*HCl, NaOAc / ethanol / 14 h / Heating
2: 56 percent / NaH / dimethylformamide / 1.) ice cooling, 30 min, 2.) room temperature, 1 h
With
hydroxylamine hydrochloride; sodium acetate; sodium hydride;
In
ethanol; N,N-dimethyl-formamide;
DOI:10.3987/COM-88-S12
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 91 percent / n-BuLi / hexane; tetrahydrofuran / 1.) ice cooling, 30 min, 2.) room temperature, 14 h
2: n-BuLi / 1.) hexane, THF, -78 deg C, 0.5 h, 2.) -78 deg C, 1 h, room temperature, 1 h
3: 85 percent / NH2OH*HCl, NaOAc / ethanol / 14 h / Heating
4: 56 percent / NaH / dimethylformamide / 1.) ice cooling, 30 min, 2.) room temperature, 1 h
With
n-butyllithium; hydroxylamine hydrochloride; sodium acetate; sodium hydride;
In
tetrahydrofuran; ethanol; hexane; N,N-dimethyl-formamide;
DOI:10.3987/COM-88-S12