fluorosulfonic acid

Base Information Edit

Chemical Name:fluorosulfonic acid
CAS No.:14483-63-7
Molecular Formula:FHO3S
Molecular Weight:122.052
Hs Code.:
Mol file:14483-63-7.mol

Synonyms:

Suppliers and Price of fluorosulfonic acid

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of fluorosulfonic acid Edit

Chemical Property:

Purity/Quality:: 99%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of fluorosulfonic acid

There total 10 articles about fluorosulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.8%

: 7789-21-1
fluorosulphonic acid

: 57-13-6
urea

: 14483-63-7
sodium fluorosulfonate

: 14984-73-7
bis(fluorosulfonyl)amide

Guidance literature:: With sodium chloride; In dichloromethane; distn. of a react.-mixt. of urea and HSO3F under vac.; distillate dissolved in CH2Cl2; NaCl added; stirred for 6 h under reflux;; NaSO3F filtered off; filtrate cooled to -80°C; filtn., recrystn. (CFCl3, -80°C).;

Reference yield: 10.0%

: 13036-75-4
fluorosulfonyl anhydride

: 13859-41-1
sodium pentacarbonyl manganate

: 640723-20-2,2699-79-8,12769-73-2
fluorosulfonyl fluoride

: 14483-63-7
sodium fluorosulfonate

: 195135-41-2
acetonitril-O,O-sulfitomanganese(II) tricarbonyl

: 201230-82-2
carbon monoxide

: 7446-09-5,12143-17-8,89125-89-3
sulfur dioxide

Guidance literature:: In acetonitrile; N2 atm.; cooling (-78°C), heating (30 min, -40°C), stirring (2 h); extraction (pentane, toluene), dissoln. (CH3CN), centrifugation, addn. of toluene; elem. anal.;

Reference yield: 5.0%

: 13036-75-4
fluorosulfonyl anhydride

: 12107-35-6
Na[CpMo(CO)3]

: 640723-20-2,2699-79-8,12769-73-2
fluorosulfonyl fluoride

: 14483-63-7
sodium fluorosulfonate

: 2Mo⁽²⁺⁾*2C₅H₅^(1-)*6CO*S₂O₅^(2-)*99CH₃CN=[Mo(C₅H₅)(CO)3(SO₂)]2O*99CH₃CN

: 201230-82-2
carbon monoxide

: 7446-09-5,12143-17-8,89125-89-3
sulfur dioxide

Guidance literature:: In methyl cyclohexane; N2 atm.; cooling (1 h, -78°C), stirring (room temp., 72 h); extraction (toluene (30°C, 30 torr), acetonitrile (vac.)), concn.(0.05 torr, 25°C), centrifugation, crystn. (PhMe/CH3CN, 10/1-1/3 );