Technology Process of 14-Pentadecynoic acid
There total 12 articles about 14-Pentadecynoic acid which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium hydroxide; water;
In
tetrahydrofuran;
at 0 - 20 ℃;
for 13h;
DOI:10.1021/ol061582d
- Guidance literature:
-
Multi-step reaction with 4 steps
1: H2 / Pd/C / methanol
2: SO3*pyridine; DMSO; (i-Pr)2NEt / CH2Cl2 / 0.5 h / 20 °C
3: 2.05 g / K2CO3 / 2 h / 20 °C
4: LiOH; H2O / tetrahydrofuran / 13 h / 0 - 20 °C
With
lithium hydroxide; pyridine-SO3 complex; water; hydrogen; potassium carbonate; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/ol061582d
- Guidance literature:
-
Multi-step reaction with 6 steps
1: SO3*pyridine; DMSO; (i-Pr)2NEt / CH2Cl2 / 0.5 h / 20 °C
2: 4.96 g / CHCl3 / 24 h / 20 °C
3: H2 / Pd/C / methanol
4: SO3*pyridine; DMSO; (i-Pr)2NEt / CH2Cl2 / 0.5 h / 20 °C
5: 2.05 g / K2CO3 / 2 h / 20 °C
6: LiOH; H2O / tetrahydrofuran / 13 h / 0 - 20 °C
With
lithium hydroxide; pyridine-SO3 complex; water; hydrogen; potassium carbonate; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; dichloromethane; chloroform;
DOI:10.1021/ol061582d
