X-ray crystal structures

a technique used to determine the three-dimensional arrangement of atoms in a crystal.

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Synthesis of tetrahydrobenzoisoquinolinols, tetrahydropyrindines, and hexahydroquinolines from 4-aryltetrahydropyridines
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- C₁₃H₁₇NO₄S
- hydrogen peroxide
- Sodium bicarbonate
Synthesis, characterization and catalytic behaviour of ansa-zirconocene complexes containing tetraphenylcyclopentadienyl rings: X-ray crystal structures of [Zr{Me₂Si(η⁵-C₅Ph₄)(η⁵-C₅H_3<
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- [Zr(Me2Si(η5-C5Ph4)(η5-C5H4))Cl2]
Insertion of ethyne into the Ru-Si bonds of coordinatively unsaturated ruthenium silyl complexes. X-ray crystal structures of Ru(CH=CHSiMe₂OEt)Cl(CO)₂(PPh₃)₂ and [Ru(CH=CHSiMe₂OH)(CN-p-tolyl)(CO)(PPh₃) ₂]ClO₄
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- Ru(-CH=CH-SiMe3)(η(2)-O2CCH3)(CO)(PPh3)2
Insertion of ethyne into the Ru-Si bonds of coordinatively unsaturated ruthenium silyl complexes. X-ray crystal structures of Ru(CH=CHSiMe₂OEt)Cl(CO)₂(PPh₃)₂ and [Ru(CH=CHSiMe₂OH)(CN-p-tolyl)(CO)(PPh₃) ₂]ClO₄
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- Ru(-CH=CH-SiMe3)(η(2)-O2CCH3)(CO)(PPh3)2
Synthesis and X-ray crystal structures of chiral, nonracemic 5,6-dihydro-4H-1,3,4-oxadiazines
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- trans-(5S,6S)-2-ethyl-4,5-dimethyl-6-phenyl-5,6-dihydro-4H-1,3,4-oxadiazine
New Modes of Bonding in Some Platinum Derivatives of B18H22: X-Ray Crystal Structures of <(Pt2B18H16)(PMe2Ph)4> and of Three Structural Isomers of <(PtB18H20)(PMe2Ph)2>
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Synthesis NMR spectra Chemical shifts Silica gel Thionyl chloride Dichloromethane Aluminum chloride Sodium bicarbonate Melting point Infrared spectra Coupling constants High resolution mass spectra Elemental analyses Cl Chiral CO Insertion Work-up and purification Reductive Amination Cyclization to Tetrahydrobenzoisoquinolinol Cyclization to Tetrahydropyrindine Cyclization to Hexahydroquinoline Catalytic Reactions Ansa-Zirconocene Complexes Tetraphenylcyclopentadienyl Rings Catalytic Behavior PPH₃ Experimental terms Ethyne Ru-Si bonds Coordinatively unsaturated Ruthenium silyl complexes CN-p-tolyl ClO₄ Ru-Si bond insertion Nonracemic 5,6-dihydro-4H-1,3,4-oxadiazines Coordination Compound Platinum derivatives B18H22 Structural isomers

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