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180635-74-9

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Basic Information
CAS No.: 180635-74-9
Name: 3-(4-TRIFLUOROMETHYL-PHENYL)-PROPAN-1-OL
Article Data: 29
Molecular Structure:
Molecular Structure of 180635-74-9 (3-(4-TRIFLUOROMETHYL-PHENYL)-PROPAN-1-OL)
Formula: C10H11 F3 O
Molecular Weight: 204.192
Synonyms: 3-(4-Trifluoromethylphenyl)-1-propanol;4-(Trifluoromethyl)benzenepropanol
Density: 1.202g/cm3
Boiling Point: 246.6°C at 760 mmHg
Flash Point: 108.1°C
PSA: 20.23000
LogP: 2.63030
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Synthetic route
53473-36-2

3-(4-trifluoromethylphenyl)propionic acid

180635-74-9

3-(4-(trifluoromethyl)phenyl)propan-1-ol

Conditions
ConditionsYield
Stage #1: 3-(4-trifluoromethylphenyl)propionic acid With borane-THF In tetrahydrofuran at 0 - 20℃; for 15.3h;
Stage #2: With methanol In tetrahydrofuran at 0℃;		100%
With borane-THF In tetrahydrofuran at 0 - 20℃; for 16h; Inert atmosphere;100%
With sodium tetrahydroborate; iodine In tetrahydrofuran at 70℃; for 16h; Cooling with ice;100%
1208-64-6

3-(4-tert-butylphenyl)propionic acid

180635-74-9

3-(4-(trifluoromethyl)phenyl)propan-1-ol

Conditions
ConditionsYield
With sodium tetrahydroborate; iodine In tetrahydrofuran at 20 - 70℃; for 16.5h; Cooling with ice;100%
455-13-0

4-Iodobenzotrifluoride

107-18-6

allyl alcohol

180635-74-9

3-(4-(trifluoromethyl)phenyl)propan-1-ol

Conditions
ConditionsYield
With potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0); tetramethylammonium formiate; triphenylphosphine In water; N,N-dimethyl-formamide at 80℃; for 4h; Heck Reaction; regioselective reaction;67%
349-95-1

4-(trifluoromethyl)benzylic alcohol

64-17-5

ethanol

180635-74-9

3-(4-(trifluoromethyl)phenyl)propan-1-ol

Conditions
ConditionsYield
With bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; potassium tert-butylate In tetrahydrofuran at 100℃; for 24h; Inert atmosphere;37%
849442-21-3

methyl 3-(4-(trifluoromethyl)phenyl)propanoate

180635-74-9

3-(4-(trifluoromethyl)phenyl)propan-1-ol

Conditions
ConditionsYield
With lithium aluminium tetrahydride In tetrahydrofuran for 3h; Heating;
With lithium aluminium tetrahydride In diethyl ether at 0℃;
With sodium tetrahydroborate In tetrahydrofuran; methanol Reflux;
455-19-6

4-Trifluoromethylbenzaldehyde

180635-74-9

3-(4-(trifluoromethyl)phenyl)propan-1-ol

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: tetrahydrofuran / Heating
2: H2 / 10 percent Pd/C / tetrahydrofuran / 2068.59 Torr
3: LiAlH4 / tetrahydrofuran / 3 h / Heating
View Scheme
20754-22-7

methyl (2E)-3-(4-(trifluoromethyl)phenyl)prop-2-enoate

180635-74-9

3-(4-(trifluoromethyl)phenyl)propan-1-ol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: H2 / 10 percent Pd/C / tetrahydrofuran / 2068.59 Torr
2: LiAlH4 / tetrahydrofuran / 3 h / Heating
View Scheme
455-13-0

4-Iodobenzotrifluoride

180635-74-9

3-(4-(trifluoromethyl)phenyl)propan-1-ol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: palladium diacetate; lithium chloride; tetrabutylammomium bromide; lithium acetate dihydrate / N,N-dimethyl-formamide / 48 h / 20 °C
2: sodium tetrahydroborate / methanol / 0.17 h / 20 °C
View Scheme
166947-09-7

3-(4-trifluoromethylphenyl)propanal

180635-74-9

3-(4-(trifluoromethyl)phenyl)propan-1-ol

Conditions
ConditionsYield
With sodium tetrahydroborate In methanol at 20℃; for 0.166667h;253 mg
173546-21-9

3-(4-trifluoromethylphenyl)prop-2-yn-1-ol

A

826994-11-0

(Z)-3-(4-(trifluoromethyl)phenyl)-2-propene-1-ol

B

125617-18-7

3-(4-trifluoromethylphenyl)-2-propen-1-ol

C

180635-74-9

3-(4-(trifluoromethyl)phenyl)propan-1-ol

Conditions
ConditionsYield
With sodium tetrahydroborate; hydrogen; cobalt(II) diacetate tetrahydrate; ethylenediamine In tetrahydrofuran; ethanol; water at 20℃; under 2250.23 Torr; for 12h; Autoclave; Glovebox; diastereoselective reaction;A n/a
B n/a
C n/a
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    Business Type:Other

    Tel:86-531-8233381 86-18678657237

    Address:Room 302,Building 1,Union Fortune Square, No. 2117,Tianchen Road,High-tech Zone,Jinan,Shandong,China

       Inquiry Now

  • Cinacalcet Impurity 29

  • Casno:

    180635-74-9

    Cinacalcet Impurity 29

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    1. Our staff are all biomedical related majors with rich experience in the pharmaceutical industry, and can provide you with more professional services.2. Our supplier has a good quality management system, and the quality of products is reliable and

  • Shenzhen Sumshine Biotech Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:15914108025

    Address:229A, No.15, Xinbeli Industrial Zone, Xinshi Community, Dalang Street, Longhua District

       Inquiry Now

  • Benzenepropanol,4-(trifluoromethyl)-

  • Casno:

    180635-74-9

    Benzenepropanol,4-(trifluoromethyl)-

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    Manufacturer,strong R&D,professional team Storage:Store in a cool, dry place. Store in a tightly closed container. Package:according to your requirement Application:ZhiShang Chemical is owned by ZhiShang Group, is a professional new-type chemicals en

  • Chemical Co.Ltd

    China (Mainland)  |  Contact Details

    Business Type:Trading Company

       Inquiry Now

  • Cinacalcet Impurity 29

  • Casno:

    180635-74-9

    Cinacalcet Impurity 29

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    High purity Application:Pharmaceutical intermediates, Material synthesis and analyzing the expectant ingredients

    Novachemistry offers a broad range of specialty chemicals and customized synthesis services to a range of pharmaceutical, agrochemical and biochemical industries. Novachemistry has

  • NovaChemistry

    United Kingdom  |  Contact Details

    Business Type:Trading Company

    Tel:+44 (0)208 191 7890

    Address:Unit11, Ark Business Centre, Gorden Road, Loughborough, United Kingdom

       Inquiry Now

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